C₂₁H₂₅NO₄S₂

Base Information

Chemical Name:C₂₁H₂₅NO₄S₂
CAS No.:915155-71-4
Molecular Formula:C₂₁H₂₅NO₄S₂
Molecular Weight:419.566
Hs Code.:

C<sub>21</sub>H<sub>25</sub>NO<sub>4</sub>S<sub>2</sub>

Synonyms:C₂₁H₂₅NO₄S₂

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Chemical Property of C₂₁H₂₅NO₄S₂

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Technology Process of C₂₁H₂₅NO₄S₂

There total 9 articles about C₂₁H₂₅NO₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: C₂₃H₁₅F₅O₅S₂

: 109-89-7
diethylamine

: 915155-71-4
C₂₁H₂₅NO₄S₂

Guidance literature:: In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ml300050b

Reference yield:

: 861108-19-2
2-(4-{4-[(2-thiiranylpropyl)sulfonyl]phenoxy}phenyl)acetic acid

: 915155-71-4
C₂₁H₂₅NO₄S₂

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C / Inert atmosphere

2: dichloromethane / 18 h / 20 °C / Inert atmosphere

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1021/ml300050b

Reference yield:

: 5656-44-0
4-(allylthio)phenol

: 915155-71-4
C₂₁H₂₅NO₄S₂

Guidance literature:: Multi-step reaction with 7 steps

1: N,N-dimethylglycine hydrochoride; caesium carbonate / copper(l) iodide / 1,4-dioxane / 22 h / 90 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 192 h / 0 - 20 °C

3: thiourea / methanol; dichloromethane / 20 °C

4: toluene / 12 h / 80 °C

5: water / acetonitrile / C₁₈-reverse phase silica gel pad

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

7: dichloromethane / 20 °C

With dmap; water; N,N-dimethylglycine hydrochoride; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; thiourea; 3-chloro-benzenecarboperoxoic acid; copper(l) iodide; In 1,4-dioxane; methanol; dichloromethane; toluene; acetonitrile; 1: Ullmann Coupling / 4: Mascaretti / 5: Mascaretti;