3-(((S)-2-hydroxy-1-phenylethyl-carbamoyl)methyl)-3-methylbutanoic acid

Base Information

Chemical Name:3-(((S)-2-hydroxy-1-phenylethyl-carbamoyl)methyl)-3-methylbutanoic acid
CAS No.:1327278-20-5
Molecular Formula:C₁₅H₂₁NO₄
Molecular Weight:279.336
Hs Code.:

Synonyms:3-(((S)-2-hydroxy-1-phenylethyl-carbamoyl)methyl)-3-methylbutanoic acid

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Chemical Property of 3-(((S)-2-hydroxy-1-phenylethyl-carbamoyl)methyl)-3-methylbutanoic acid

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Technology Process of 3-(((S)-2-hydroxy-1-phenylethyl-carbamoyl)methyl)-3-methylbutanoic acid

There total 1 articles about 3-(((S)-2-hydroxy-1-phenylethyl-carbamoyl)methyl)-3-methylbutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 4160-82-1
3,3-dimethylglutaric anhydride

: 20989-17-7
(2S)-2-phenylglycinol

: 1327278-20-5
3-(((S)-2-hydroxy-1-phenylethyl-carbamoyl)methyl)-3-methylbutanoic acid

Guidance literature:: In dichloromethane; toluene; at 20 - 60 ℃; for 5.5h;
DOI:10.1002/asia.201100452

Reference yield: 83.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1327278-20-5
3-(((S)-2-hydroxy-1-phenylethyl-carbamoyl)methyl)-3-methylbutanoic acid

: 1327277-98-4
(S)-methyl 5-((2-hydroxy-1-phenylethyl)amino)-3,3-dimethyl-5-oxopentanoate

Guidance literature:: In methanol; diethyl ether; at 0 - 20 ℃;
DOI:10.1002/asia.201100452

Reference yield:

: 1327278-20-5
3-(((S)-2-hydroxy-1-phenylethyl-carbamoyl)methyl)-3-methylbutanoic acid

: 1327278-03-4
methyl 3-(((S)-4,5-dihydro-4-phenyloxazol-2-yl)methyl)-3-methylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol; diethyl ether / 0 - 20 °C

2.1: trichlorophosphate / toluene / 2 h / 20 °C

2.2: 0.75 h

With trichlorophosphate; In methanol; diethyl ether; toluene;
DOI:10.1002/asia.201100452