(S)-methyl 5-((2-hydroxy-1-phenylethyl)amino)-3,3-dimethyl-5-oxopentanoate

Base Information

Chemical Name:(S)-methyl 5-((2-hydroxy-1-phenylethyl)amino)-3,3-dimethyl-5-oxopentanoate
CAS No.:1327277-98-4
Molecular Formula:C₁₆H₂₃NO₄
Molecular Weight:293.363
Hs Code.:

Synonyms:(S)-methyl 5-((2-hydroxy-1-phenylethyl)amino)-3,3-dimethyl-5-oxopentanoate

Suppliers and Price of (S)-methyl 5-((2-hydroxy-1-phenylethyl)amino)-3,3-dimethyl-5-oxopentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-methyl 5-((2-hydroxy-1-phenylethyl)amino)-3,3-dimethyl-5-oxopentanoate

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Technology Process of (S)-methyl 5-((2-hydroxy-1-phenylethyl)amino)-3,3-dimethyl-5-oxopentanoate

There total 3 articles about (S)-methyl 5-((2-hydroxy-1-phenylethyl)amino)-3,3-dimethyl-5-oxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1327278-20-5
3-(((S)-2-hydroxy-1-phenylethyl-carbamoyl)methyl)-3-methylbutanoic acid

: 1327277-98-4
(S)-methyl 5-((2-hydroxy-1-phenylethyl)amino)-3,3-dimethyl-5-oxopentanoate

Guidance literature:: In methanol; diethyl ether; at 0 - 20 ℃;
DOI:10.1002/asia.201100452

Reference yield:

: 4160-82-1
3,3-dimethylglutaric anhydride

: 1327277-98-4
(S)-methyl 5-((2-hydroxy-1-phenylethyl)amino)-3,3-dimethyl-5-oxopentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane; toluene / 5.5 h / 20 - 60 °C

2: methanol; diethyl ether / 0 - 20 °C

In methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1002/asia.201100452

Reference yield:

: 20989-17-7
(2S)-2-phenylglycinol

: 1327277-98-4
(S)-methyl 5-((2-hydroxy-1-phenylethyl)amino)-3,3-dimethyl-5-oxopentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane; toluene / 5.5 h / 20 - 60 °C

2: methanol; diethyl ether / 0 - 20 °C

In methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1002/asia.201100452