Technology Process of C17H15N3O3
There total 5 articles about C17H15N3O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C19H19N3O3;
With
water; sodium hydroxide;
In
tetrahydrofuran; ethanol;
at 20 ℃;
for 2h;
Cooling with ice;
With
hydrogenchloride;
In
tetrahydrofuran; ethanol; water;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene-4-sulfonic acid; hydrazine hydrate / 21 h / 120 °C / Cooling with ice
2.1: potassium hydroxide; iodine / N,N-dimethyl-formamide / 1 h / 20 °C / Cooling with ice
3.1: sodium hydride / N,N-dimethyl-formamide / 3 h / Cooling with ice
3.2: 1 h / 20 °C / Cooling with ice
4.1: triethylamine / triphenylphosphine; palladium diacetate / 1,4-dioxane / 4 h / 100 °C / Inert atmosphere
5.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 2 h / 20 °C / Cooling with ice
5.2: Cooling with ice
With
water; iodine; sodium hydride; toluene-4-sulfonic acid; hydrazine hydrate; triethylamine; potassium hydroxide; sodium hydroxide;
palladium diacetate; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 3 h / Cooling with ice
1.2: 1 h / 20 °C / Cooling with ice
2.1: triethylamine / triphenylphosphine; palladium diacetate / 1,4-dioxane / 4 h / 100 °C / Inert atmosphere
3.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 2 h / 20 °C / Cooling with ice
3.2: Cooling with ice
With
water; sodium hydride; triethylamine; sodium hydroxide;
palladium diacetate; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl-formamide;