Formic acid 1-((1S,2S,7aR)-1-benzyloxymethyl-5-oxo-hexahydro-pyrrolizin-2-yl)-1-methyl-ethyl ester

Base Information

• Chemical Name: Formic acid 1-((1S,2S,7aR)-1-benzyloxymethyl-5-oxo-hexahydro-pyrrolizin-2-yl)-1-methyl-ethyl ester
• CAS No.: 83004-57-3
• Molecular Formula: C₁₉H₂₅NO₄
• Molecular Weight: 331.412

Synonyms:Formic acid 1-((1S,2S,7aR)-1-benzyloxymethyl-5-oxo-hexahydro-pyrrolizin-2-yl)-1-methyl-ethyl ester

Chemical Property of Formic acid 1-((1S,2S,7aR)-1-benzyloxymethyl-5-oxo-hexahydro-pyrrolizin-2-yl)-1-methyl-ethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of Formic acid 1-((1S,2S,7aR)-1-benzyloxymethyl-5-oxo-hexahydro-pyrrolizin-2-yl)-1-methyl-ethyl ester

There total 2 articles about Formic acid 1-((1S,2S,7aR)-1-benzyloxymethyl-5-oxo-hexahydro-pyrrolizin-2-yl)-1-methyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N-((E)-5-Benzyloxy-2,2-dimethyl-pent-3-enyl)-3-[1,3]dioxan-2-yl-propionamide (83004-73-3) → (6R,7R,7aS)-7-Benzyloxymethyl-6-isopropyl-hexahydro-pyrrolizin-3-one + Formic acid 1-((1S,2S,7aR)-1-benzyloxymethyl-5-oxo-hexahydro-pyrrolizin-2-yl)-1-methyl-ethyl ester (83004-57-3) + Formic acid (7R,8R,8aS)-8-benzyloxymethyl-6,6-dimethyl-3-oxo-octahydro-indolizin-7-yl ester (83004-56-2)

Guidance literature:

In formic acid; for 21h; Ambient temperature;

DOI:10.1016/S0040-4039(00)87451-1

Reference yield: 10.0%

formic acid (64-18-6) + N-((E)-5-Benzyloxy-2,2-dimethyl-pent-3-enyl)-3-[1,3]dioxan-2-yl-propionamide (83004-73-3) → (6R,7R,7aS)-7-Benzyloxymethyl-6-isopropyl-hexahydro-pyrrolizin-3-one + Formic acid 1-((1S,2S,7aR)-1-benzyloxymethyl-5-oxo-hexahydro-pyrrolizin-2-yl)-1-methyl-ethyl ester (83004-57-3) + Formic acid (7R,8R,8aS)-8-benzyloxymethyl-6,6-dimethyl-3-oxo-octahydro-indolizin-7-yl ester (83004-56-2)

Guidance literature:

for 21h; Ambient temperature;

DOI:10.1016/S0040-4039(00)87451-1

Reference yield: 94.0%

Formic acid 1-((1S,2S,7aR)-1-benzyloxymethyl-5-oxo-hexahydro-pyrrolizin-2-yl)-1-methyl-ethyl ester (83004-57-3) → (6R,7R,7aS)-7-Benzyloxymethyl-6-isopropyl-hexahydro-pyrrolizin-3-one

Guidance literature:

With sodium hydroxide; In methanol; water;

DOI:10.1016/S0040-4039(00)87451-1

upstream raw materials:

formic acid

N-((E)-5-Benzyloxy-2,2-dimethyl-pent-3-enyl)-3-[1,3]dioxan-2-yl-propionamide

Downstream raw materials:

(+/-)-supinidine

(7S,7aR)-7-Benzyloxymethyl-hexahydro-pyrrolizin-3-one

(7S,7aR)-7-Benzyloxymethyl-6-iodo-hexahydro-pyrrolizin-3-one

benzaldehyde

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