2,4-dichloro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methylamino]phenol

Base Information

Chemical Name:2,4-dichloro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methylamino]phenol
CAS No.:1427407-34-8
Molecular Formula:C₁₉H₁₃Cl₂F₂NO
Molecular Weight:380.221
Hs Code.:

Synonyms:2,4-dichloro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methylamino]phenol

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Chemical Property of 2,4-dichloro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methylamino]phenol

Chemical Property:

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Technology Process of 2,4-dichloro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methylamino]phenol

There total 9 articles about 2,4-dichloro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methylamino]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1427407-33-7
2,6-dichloro-N-[[2-fluoro-5-(3-fluorophenyl)phenyl]methyl]-3-methoxyaniline

: 1427407-34-8
2,4-dichloro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methylamino]phenol

Guidance literature:: With boron tribromide; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 1214382-15-6
C₁₃H₇ClF₂O

: 1427407-34-8
2,4-dichloro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methylamino]phenol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran / 2 h / 20 °C

2: borane-THF / tetrahydrofuran / 60 °C

3: boron tribromide / dichloromethane / 0 - 20 °C

With borane-THF; boron tribromide; sodium hydride; In tetrahydrofuran; dichloromethane;

Reference yield:

: 38902-87-3
3-nitro-2,4-dichlorophenol

: 1427407-34-8
2,4-dichloro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methylamino]phenol

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetone / 0.5 h / 20 °C

1.2: 20 °C

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate

3.1: sodium hydride / tetrahydrofuran / 2 h / 20 °C

4.1: borane-THF / tetrahydrofuran / 60 °C

5.1: boron tribromide / dichloromethane / 0 - 20 °C

With borane-THF; palladium 10% on activated carbon; hydrogen; boron tribromide; sodium hydride; potassium carbonate; In tetrahydrofuran; dichloromethane; ethyl acetate; acetone;