C₁₁H₁₂NO₃^(1-)*Na⁽¹⁺⁾

Base Information

• Chemical Name: C₁₁H₁₂NO₃^(1-)*Na⁽¹⁺⁾
• CAS No.: 108306-69-0
• Molecular Formula: C₁₁H₁₂NO₃*Na
• Molecular Weight: 229.211
• Mol file: 108306-69-0.mol

Synonyms:C₁₁H₁₂NO₃^(1-)*Na⁽¹⁺⁾

Chemical Property of C₁₁H₁₂NO₃^(1-)*Na⁽¹⁺⁾

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₁H₁₂NO₃^(1-)*Na⁽¹⁺⁾

There total 4 articles about C₁₁H₁₂NO₃^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

propan-1-ol (71-23-8) + 3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole> (108306-66-7) → N,N'-ethylenethiourea (96-45-7) + C11H12NO3(1-)*Na(1+) (108306-69-0)

Guidance literature:

With sodium hydroxide; at 20 ℃; for 0.333333h;

DOI:10.1055/s-1986-33422

Reference yield:

1-(N-Benzoylthiocarbamoyl)-2-imidazolidinethione (108324-95-4) → C11H12NO3(1-)*Na(1+) (108306-69-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 84 percent / conc. HCl, 30percent H₂O₂ / ethanol / 0.08 h / Heating

2: 80 percent / 25percent aq. NH₄OH / ethanol / 20 °C

3: 71 percent / NaOH / 0.33 h / 20 °C

With hydrogenchloride; ammonium hydroxide; sodium hydroxide; dihydrogen peroxide; In ethanol;

DOI:10.1055/s-1986-33422

Reference yield:

Benzoyl isothiocyanate (532-55-8) → C11H12NO3(1-)*Na(1+) (108306-69-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 56 percent / acetone / 4 h / Heating

2: 84 percent / conc. HCl, 30percent H₂O₂ / ethanol / 0.08 h / Heating

3: 80 percent / 25percent aq. NH₄OH / ethanol / 20 °C

4: 71 percent / NaOH / 0.33 h / 20 °C

With hydrogenchloride; ammonium hydroxide; sodium hydroxide; dihydrogen peroxide; In ethanol; acetone;

DOI:10.1055/s-1986-33422

upstream raw materials:

propan-1-ol

3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole>

1-(N-Benzoylthiocarbamoyl)-2-imidazolidinethione

3-Benzoylimino-5,6-dihydro-3H<1,2,4>dithiazole> hydrochloride

Downstream raw materials:

O-Propyl-N-benzoylcarbamate