dicarbonyl(pentamethylcyclopentadienyl)phenyliron

Base Information

Chemical Name:dicarbonyl(pentamethylcyclopentadienyl)phenyliron
CAS No.:43157-73-9
Molecular Formula:C₁₈H₂₀FeO₂
Molecular Weight:324.203
Hs Code.:

Synonyms:dicarbonyl(pentamethylcyclopentadienyl)phenyliron

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Chemical Property of dicarbonyl(pentamethylcyclopentadienyl)phenyliron

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Technology Process of dicarbonyl(pentamethylcyclopentadienyl)phenyliron

There total 6 articles about dicarbonyl(pentamethylcyclopentadienyl)phenyliron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: iodo(η5-pentamethylcyclopentadienyl)iron dicarbonyl

: 960-16-7
tributylphenylstannane

: 43157-73-9
dicarbonyl(pentamethylcyclopentadienyl)phenyliron

Guidance literature:: With copper(I) triflate; In 1,4-dioxane; at 60 ℃; for 4h; Inert atmosphere;
DOI:10.1021/om301219t

Reference yield:

: {bis(triphenylphosphine)nitrogen}{BPh₄}

: [(η5-C5Me5)Fe(CO)2(BC6H2Me3-2,4,6)][B(C6H3(CF3)2-3,5)4]

: 43157-73-9
dicarbonyl(pentamethylcyclopentadienyl)phenyliron

: 960-71-4
triphenylborane

Guidance literature:: In dichloromethane; under inert atm. soln. (Cp*Fe(CO)2B(Mes))(BAr4) in CH2Cl2 at -78°C was added to soln. (PPN)BPh4 in CH2Cl2, react. mixt. was warmed slowlyto room temp. and stirred for 1 h; volatiles were removed in vacuo, residue was extd. with hexane and cooled to -50°C;
DOI:10.1021/om049793e

Reference yield:

: 501122-91-4
(η5-C5Me5)Fe(CO)2B(2,4,6-Me3C6H2)Br

: 143-66-8
sodium tetraphenyl borate

: 43157-73-9
dicarbonyl(pentamethylcyclopentadienyl)phenyliron

: 960-71-4
triphenylborane

Guidance literature:: In dichloromethane; under inert atm. soln. Cp*Fe(CO)2B(Mes)Br in CH2Cl2 at -78°C was added to suspn. NaBPh4 in CH2Cl2, react. mixt. was warmed slowly to roomtemp.; volatiles were removed in vacuo, residue was extd. with hexane and cooled to -50°C;
DOI:10.1021/om049793e