(2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:(2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-β-D-glucopyranoside
CAS No.:1334540-35-0
Molecular Formula:C₂₄H₃₀O₅S
Molecular Weight:430.565
Hs Code.:

Synonyms:(2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Suppliers and Price of (2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

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Technology Process of (2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

There total 5 articles about (2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 1421758-31-7
(2-methyl-5-tert-butylphenyl) 1-thio-β-D-glucopyranoside

: 1334540-35-0
(2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: With 10-camphorsulfonic acid; In acetonitrile; Inert atmosphere;
DOI:10.1002/chem.201204518

Reference yield:

: 1421758-31-7
(2-methyl-5-tert-butylphenyl) 1-thio-β-D-glucopyranoside

: 100-52-7
benzaldehyde

: 1334540-35-0
(2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: With 1,1-dimethoxyethane; camphor-10-sulfonic acid; In acetonitrile; at 20 ℃; for 2.5h; regioselective reaction; Ionic liquid;

Reference yield:

: 7340-90-1
2-methyl-5-tert-butylthiophenol

: 1334540-35-0
(2-methyl-5-tert-butylphenyl) 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane

2: sodium methylate / methanol / 20 °C

3: camphor-10-sulfonic acid / acetonitrile / 2.5 h / 20 °C / Inert atmosphere

With camphor-10-sulfonic acid; boron trifluoride diethyl etherate; sodium methylate; In methanol; dichloromethane; acetonitrile;
DOI:10.1039/c1cc13614c