H₂N-DEG-CH₂CONH-Gly-Phe-Leu-Gly-EDADNS

Base Information

Chemical Name:H₂N-DEG-CH₂CONH-Gly-Phe-Leu-Gly-EDADNS
CAS No.:1321923-28-7
Molecular Formula:C₃₉H₅₆N₈O₉S
Molecular Weight:812.988
Hs Code.:

H<sub>2</sub>N-DEG-CH<sub>2</sub>CONH-Gly-Phe-Leu-Gly-EDADNS

Synonyms:H₂N-DEG-CH₂CONH-Gly-Phe-Leu-Gly-EDADNS

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Chemical Property of H₂N-DEG-CH₂CONH-Gly-Phe-Leu-Gly-EDADNS

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Technology Process of H₂N-DEG-CH₂CONH-Gly-Phe-Leu-Gly-EDADNS

There total 15 articles about H₂N-DEG-CH₂CONH-Gly-Phe-Leu-Gly-EDADNS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1321923-38-9
FmocNH-DEG-CH₂CONH-Gly-Phe-Leu-Gly-EDADNS

: 1321923-28-7
H₂N-DEG-CH₂CONH-Gly-Phe-Leu-Gly-EDADNS

Guidance literature:: With diethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere; Darkness;
DOI:10.1021/ja204488p

Reference yield:

: 6338-55-2
2-(2-(2-aminoethoxy)ethoxy)ethan-1-ol

: 1321923-28-7
H₂N-DEG-CH₂CONH-Gly-Phe-Leu-Gly-EDADNS

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydrogencarbonate / water / Inert atmosphere

2.1: sodium hypochlorite; 2,2,6,6-tetramethyl-piperidine-N-oxyl / dichloromethane / Inert atmosphere

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.33 h / -15 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: 5%-palladium/activated carbon; hydrogen / ethanol; ethyl acetate / 2 h / 760.05 Torr / Inert atmosphere

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.33 h / -15 °C / Inert atmosphere; Darkness

5.2: 20 °C / Inert atmosphere; Darkness

6.1: diethylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere; Darkness

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; 5%-palladium/activated carbon; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; In ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ja204488p

Reference yield:

: 200427-89-0
t-butyloxycarbonyl-glycyl-phenyl-leucyl-glycyl-O-benzyl ester

: 1321923-28-7
H₂N-DEG-CH₂CONH-Gly-Phe-Leu-Gly-EDADNS

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / 3 h / 20 °C / Inert atmosphere

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.33 h / -15 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: 5%-palladium/activated carbon; hydrogen / ethanol; ethyl acetate / 2 h / 760.05 Torr / Inert atmosphere

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.33 h / -15 °C / Inert atmosphere; Darkness

4.2: 20 °C / Inert atmosphere; Darkness

5.1: diethylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere; Darkness

With 5%-palladium/activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; In ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ja204488p