di-μ-bromobis(N-methyl-3,4-dimethoxybenzalimine-6,C,N)dipalladium(II)

Base Information

Chemical Name:di-μ-bromobis(N-methyl-3,4-dimethoxybenzalimine-6,C,N)dipalladium(II)
CAS No.:89506-15-0
Molecular Formula:C₂₀H₂₄Br₂N₂O₄Pd₂
Molecular Weight:729.07
Hs Code.:

Synonyms:di-μ-bromobis(N-methyl-3,4-dimethoxybenzalimine-6,C,N)dipalladium(II)

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Chemical Property of di-μ-bromobis(N-methyl-3,4-dimethoxybenzalimine-6,C,N)dipalladium(II)

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Technology Process of di-μ-bromobis(N-methyl-3,4-dimethoxybenzalimine-6,C,N)dipalladium(II)

There total 1 articles about di-μ-bromobis(N-methyl-3,4-dimethoxybenzalimine-6,C,N)dipalladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 89525-44-0
N-methyl-3,4-dimethoxy-6-bromobenzalimine

: 32005-36-0
bis(dibenzylideneacetone)-palladium⁽⁰⁾

: 89506-15-0
di-μ-bromobis(N-methyl-3,4-dimethoxybenzalimine-6,C,N)dipalladium(II)

Guidance literature:: In benzene; byproducts: Pd; org. educt added to stirred soln. of complex in dry C6H6 at room temp. under N2, heated slowly to 60°C, heated for 5 min; collected at room temp., washed with C6H6, dried;
DOI:10.1016/0022-328X(84)80664-6

Reference yield: 95.0%

: 89506-15-0
di-μ-bromobis(N-methyl-3,4-dimethoxybenzalimine-6,C,N)dipalladium(II)

: 89506-21-8
bromo(N-methyl-3,4-dimethoxybenzalimine-6,C,N)triphenylphosphinepalladium(II)

Guidance literature:: With triphenylphosphine; In dichloromethane; byproducts: Pd; PPh3 and complex stirred at room temp. in CH2Cl2; filtered (celite), heated, pptd. (MeOH), filtered, washed (MeOH), dried; elem. anal.;
DOI:10.1016/0022-328X(84)80664-6