[chlorido{3-(oxo-.κappa.O)-2-phenyl-chromen-4(1H)-onato-.κappa.O}(η6-p-cymene)ruthenium(II)]

Base Information

• Chemical Name: [chlorido{3-(oxo-.κappa.O)-2-phenyl-chromen-4(1H)-onato-.κappa.O}(η6-p-cymene)ruthenium(II)]
• CAS No.: 1376044-08-4
• Molecular Formula: C₂₅H₂₃ClO₃Ru
• Molecular Weight: 507.979

Synonyms:[chlorido{3-(oxo-.κappa.O)-2-phenyl-chromen-4(1H)-onato-.κappa.O}(η6-p-cymene)ruthenium(II)]

Chemical Property of [chlorido{3-(oxo-.κappa.O)-2-phenyl-chromen-4(1H)-onato-.κappa.O}(η6-p-cymene)ruthenium(II)]

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Technology Process of [chlorido{3-(oxo-.κappa.O)-2-phenyl-chromen-4(1H)-onato-.κappa.O}(η6-p-cymene)ruthenium(II)]

There total 2 articles about [chlorido{3-(oxo-.κappa.O)-2-phenyl-chromen-4(1H)-onato-.κappa.O}(η6-p-cymene)ruthenium(II)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 (52462-29-0) + 3-hydroxyflavone (577-85-5,66585-05-5) → [chlorido{3-(oxo-.κappa.O)-2-phenyl-chromen-4(1H)-onato-.κappa.O}(η6-p-cymene)ruthenium(II)] (1376044-08-4)

Guidance literature:

3-hydroxyflavone; With lithium hexamethyldisilazane; In diethyl ether; at 20 ℃; for 3h; Glovebox; Inert atmosphere;

[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; In acetonitrile; Glovebox; Inert atmosphere;

DOI:10.1021/om5006337

Reference yield: 51.0%

[RhCl2(p-cymene)]2 + 3-hydroxyflavone (577-85-5,66585-05-5) → [chlorido{3-(oxo-.κappa.O)-2-phenyl-chromen-4(1H)-onato-.κappa.O}(η6-p-cymene)ruthenium(II)] (1376044-08-4)

Guidance literature:

With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1021/jm301376a

Reference yield: 86.0%

[chlorido{3-(oxo-.κappa.O)-2-phenyl-chromen-4(1H)-onato-.κappa.O}(η6-p-cymene)ruthenium(II)] (1376044-08-4) + silver trifluoromethanesulfonate (2923-28-6) + acetonitrile (75-05-8,26809-02-9) → [Ru(η6-p-cymene)(3-Hfl)]OTf

Guidance literature:

at 20 ℃; for 3h; Inert atmosphere; Glovebox;

DOI:10.1021/om5006337

upstream raw materials:

[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

3-hydroxyflavone

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