4-(2-(benzyloxy)phenyl)-2-(4-methoxyphenyl)-1-tosyl-1,4-dihydroquinoline

Base Information

Chemical Name:4-(2-(benzyloxy)phenyl)-2-(4-methoxyphenyl)-1-tosyl-1,4-dihydroquinoline
CAS No.:1447235-36-0
Molecular Formula:C₃₆H₃₁NO₄S
Molecular Weight:573.712
Hs Code.:

Synonyms:4-(2-(benzyloxy)phenyl)-2-(4-methoxyphenyl)-1-tosyl-1,4-dihydroquinoline

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Chemical Property of 4-(2-(benzyloxy)phenyl)-2-(4-methoxyphenyl)-1-tosyl-1,4-dihydroquinoline

Chemical Property:

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Technology Process of 4-(2-(benzyloxy)phenyl)-2-(4-methoxyphenyl)-1-tosyl-1,4-dihydroquinoline

There total 4 articles about 4-(2-(benzyloxy)phenyl)-2-(4-methoxyphenyl)-1-tosyl-1,4-dihydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1447235-06-4
(E)-N-((E)-3-(2-(benzyloxy)phenyl)-1-(4-methoxyphenyl)allylidene)-4-methylbenzenesulfonamide

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 1447235-36-0
4-(2-(benzyloxy)phenyl)-2-(4-methoxyphenyl)-1-tosyl-1,4-dihydroquinoline

Guidance literature:: anthranilic acid; With isopentyl nitrite; trichloroacetic acid; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

(E)-N-((E)-3-(2-(benzyloxy)phenyl)-1-(4-methoxyphenyl)allylidene)-4-methylbenzenesulfonamide; With 2-methyl-1,2-epoxypropane; In chlorobenzene; Reflux;
DOI:10.1080/00397911.2012.726388

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1447235-36-0
4-(2-(benzyloxy)phenyl)-2-(4-methoxyphenyl)-1-tosyl-1,4-dihydroquinoline

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / ethanol / 20 °C

2.1: titanium tetrachloride; triethylamine / dichloromethane; 1,2-dichloro-ethane / Reflux

3.1: trichloroacetic acid; isopentyl nitrite / tetrahydrofuran / 1 h / 0 - 20 °C

3.2: Reflux

With titanium tetrachloride; triethylamine; potassium hydroxide; isopentyl nitrite; trichloroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1080/00397911.2012.726388

Reference yield:

: 5896-17-3
2-(phenylmethoxy)benzaldehyde

: 1447235-36-0
4-(2-(benzyloxy)phenyl)-2-(4-methoxyphenyl)-1-tosyl-1,4-dihydroquinoline

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / ethanol / 20 °C

2.1: titanium tetrachloride; triethylamine / dichloromethane; 1,2-dichloro-ethane / Reflux

3.1: trichloroacetic acid; isopentyl nitrite / tetrahydrofuran / 1 h / 0 - 20 °C

3.2: Reflux

With titanium tetrachloride; triethylamine; potassium hydroxide; isopentyl nitrite; trichloroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1080/00397911.2012.726388