N-benzyl-N-isopropylallylamine

Base Information

• Chemical Name: N-benzyl-N-isopropylallylamine
• CAS No.: 247033-00-7
• Molecular Formula: C₁₃H₁₉N
• Molecular Weight: 189.301
• Mol file: 247033-00-7.mol

Synonyms:N-benzyl-N-isopropylallylamine

Chemical Property of N-benzyl-N-isopropylallylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzyl-N-isopropylallylamine

There total 2 articles about N-benzyl-N-isopropylallylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

Benzyl-isopropyl-amin (102-97-6) + allyl alcohol (107-18-6) → N-benzyl-N-isopropylallylamine (247033-00-7)

Guidance literature:

With ammonium hexafluorophosphate; [Pt(η3-C3H5)(DPP-Xantphos)]PF6; In toluene; acetonitrile; at 50 ℃; for 8h; Inert atmosphere;

DOI:10.1002/chem.200801197

Reference yield: 93.0%

Benzyl-isopropyl-amin (102-97-6) + allyl bromide (106-95-6) → N-benzyl-N-isopropylallylamine (247033-00-7)

Guidance literature:

With sodium hydroxide; In N,N-dimethyl-formamide; for 1h; Ambient temperature;

DOI:10.1016/S0957-4166(99)00248-7

Reference yield:

N-benzyl-N-isopropylallylamine (247033-00-7) → (S)-1-isopropylamino-3-(1-naphthyloxy)-2-propanol (4199-09-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) Li₂PdCl₄, CuCl₂, 2.) aq. CF₃COOH, 3.) Na₂S*9H₂O

3: 86 percent / Et₃N / Heating

4: 100 percent / H₂ / 10 percent Pd/C / ethanol / 24 h / 25 °C / 3040 Torr

With sodium sulfide; lithium tetrachloropalladate(II); hydrogen; triethylamine; trifluoroacetic acid; copper dichloride; palladium on activated charcoal; In ethanol;

DOI:10.1016/S0957-4166(99)00248-7

upstream raw materials:

Benzyl-isopropyl-amin

allyl bromide

allyl alcohol

Downstream raw materials:

N-benzyl-N-isopropyl-2,3-epoxypropylamine

(S)-1-isopropylamino-3-(1-naphthyloxy)-2-propanol

(2S)-1-(isopropylamino)-3-(2-methoxyphenoxy)propan-2-ol

Acetic acid (R)-1-acetoxymethyl-2-(benzyl-isopropyl-amino)-ethyl ester