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Isopropylbenzylamine Crystals BenzylisopropylamineCAS 102-97-6
Cas No: 102-97-6
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Cas No: 102-97-6
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High purity N-Benzylisopropylamine
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102-97-6 Usage

Chemical Properties

CLEAR VERY SLIGHTLY YELLOW TO YELLOW LIQUID
InChI:InChI=1/C10H15N/c1-9(2)11-8-10-6-4-3-5-7-10/h3-7,9,11H,8H2,1-2H3/p+1

102-97-6 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (B23243)  N-Isopropylbenzylamine, 97%    102-97-6 500g 1137.0CNY Detail
Alfa Aesar (B23243)  N-Isopropylbenzylamine, 97%    102-97-6 100g 375.0CNY Detail

102-97-6SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name N-Benzylisopropylamine

1.2 Other means of identification

Product number -
Other names N-Benzylpropan-2-amine

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:102-97-6 SDS

102-97-6Synthetic route

isopropyl alcohol
67-63-0

isopropyl alcohol

benzylamine
100-46-9

benzylamine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With C13H20N2O*Ir(1+); hydrogen at 80℃; under 3000.3 Torr; for 23h; Reagent/catalyst; Autoclave; Green chemistry;100%
With nickel at 20℃; for 26h;70%
Pt on TiO2 for 10h; Ambient temperature; Irradiation;36.32%
1-benzyl-2-(chloromethyl)aziridine

1-benzyl-2-(chloromethyl)aziridine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether for 6h; Reflux;98%
diisopropylamine
108-18-9

diisopropylamine

benzylamine
100-46-9

benzylamine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With μ-diiodo-di((η5-pentamethylcyclopentadienyl)(iodo)iridium) In 5,5-dimethyl-1,3-cyclohexadiene at 155℃; for 10h; Inert atmosphere;97%
With [(C5Me4)(CH2)3(C5Me4)(IrI2)2]m In 5,5-dimethyl-1,3-cyclohexadiene at 155℃; for 10h; Schlenk technique; Reflux;96%
N-isopropylbenzamide
5440-69-7

N-isopropylbenzamide

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
Stage #1: N-isopropylbenzamide With 2-fluoropyridine; trifluoromethylsulfonic anhydride In dichloromethane at 0℃; for 0.333333h;
Stage #2: With 1,1,3,3-Tetramethyldisiloxane In dichloromethane at 0 - 20℃; for 3.16667h;
Stage #3: With tris(pentafluorophenyl)borate In dichloromethane at 0 - 20℃;
94%
With lithium aluminium tetrahydride In diethyl ether for 5h; Heating;
With diphenylsilane; triphenylphosphine; chloro(1,5-cyclooctadiene)rhodium(I) dimer In tetrahydrofuran at 20℃; for 48h;80 % Spectr.
(E)-N-benzylidenepropan-2-amine
27845-51-8

(E)-N-benzylidenepropan-2-amine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With titanocene dichloride; butyl magnesium bromide In diethyl ether at 25℃; for 15h; Mechanism; var. aldimine and cyclic ketimine substr.; var. quant. of catalyst;94%
With titanocene dichloride; butyl magnesium bromide In diethyl ether at 25℃; for 15h;94%
N-benzylideneisopropylamine
6852-56-8

N-benzylideneisopropylamine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With sodium tetrahydroborate; (-) In ethanol at 20℃; for 72h;92%
With ammonia borane at 20℃; for 12h;75%
With sodium tetrahydroborate In methanol at 20℃; for 1h;
benzaldehyde
100-52-7

benzaldehyde

isopropylamine
75-31-0

isopropylamine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With bis(benzonitrile)palladium(II) dichloride; hydrogen; 2,2′‐biquinoline‐4,4′‐dicarboxylic acid dipotassium salt at 100℃; under 10343 Torr; for 24h;90%
With sodium tetrahydroborate In 2,2,2-trifluoroethanol at 35 - 40℃; for 0.0333333h;90%
Stage #1: benzaldehyde; isopropylamine In tetrahydrofuran; methanol for 6h; Molecular sieve;
Stage #2: With sodium tetrahydroborate In tetrahydrofuran; methanol at 0 - 20℃; for 2h;
85%
acetone
67-64-1

acetone

benzylamine
100-46-9

benzylamine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With iridium bromide; sulfuric acid; zinc In 1,4-dioxane; water at 30℃; for 72h;88%
With sodium hydrogen telluride In ethanol for 20h; Ambient temperature;80%
With sodium tris(acetoxy)borohydride In dichloromethane at 30℃;70%
benzyldiisopropylamine
34636-09-4

benzyldiisopropylamine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With iodine; sodium carbonate In chloroform at 60℃; for 24h;86%
benzyl chloride
100-44-7

benzyl chloride

isopropylamine
75-31-0

isopropylamine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With copper(l) chloride In ethanol at 40℃; Reagent/catalyst; Solvent; Temperature;85.3%
With sodium carbonate In glycerol
N-benzyl-2-(bromomethyl)aziridine
25662-24-2

N-benzyl-2-(bromomethyl)aziridine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether Reflux;82%
benzaldehyde
100-52-7

benzaldehyde

Isopropylamine hydroperchlorate
15576-36-0

Isopropylamine hydroperchlorate

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With tri-n-butyl-tin hydride In N,N-dimethyl-formamide at 20℃; for 4h; Reductive amination;73%
benzyldiisopropylamine
34636-09-4

benzyldiisopropylamine

methylphenylsilane
766-08-5

methylphenylsilane

A

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

B

methyl(phenyl)(1-propyl)silane

methyl(phenyl)(1-propyl)silane

Conditions
ConditionsYield
With tris(pentafluorophenyl)borate In chlorobenzene at 130℃; for 36h; Inert atmosphere; Glovebox;A 70%
B 36%
(Z)‑N‑isopropyl‑1‑phenylmethanimine oxide
10229-64-8, 143957-81-7, 300802-10-2

(Z)‑N‑isopropyl‑1‑phenylmethanimine oxide

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With 4,4'-di-tert-butylbiphenyl; lithium; nickel dichloride In tetrahydrofuran at 20℃; for 6h;67%
N-benzyl-4-methylbenzenesulfinamide
6873-90-1

N-benzyl-4-methylbenzenesulfinamide

isopropyl alcohol
67-63-0

isopropyl alcohol

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With nickel at 20℃; for 6h;65%
acetone
67-64-1

acetone

Benzaldoxime
932-90-1

Benzaldoxime

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With hydrogen; magnesium oxide; copper at 220℃; under 11250.9 Torr;61%
diisopropylamine
108-18-9

diisopropylamine

dibenzylamine
103-49-1

dibenzylamine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With μ-diiodo-di((η5-pentamethylcyclopentadienyl)(iodo)iridium) In 5,5-dimethyl-1,3-cyclohexadiene at 155℃; for 10h; Inert atmosphere;60%
(E)-N-benzylidenepropan-2-amine
27845-51-8

(E)-N-benzylidenepropan-2-amine

A

N,N'-diisopropyl-1,2-diphenyl-1,2-ethanediamine
55079-98-6

N,N'-diisopropyl-1,2-diphenyl-1,2-ethanediamine

B

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With sodium hydroxide; zinc In water for 5.2h; Ambient temperature;A 20%
B 53%
With samarium diiodide In tetrahydrofuran at 180℃; under 8250.66 - 10500.8 Torr; for 0.0833333h; Product distribution; Further Variations:; Reagents; time; microwave irradiation;
benzyl bromide
100-39-0

benzyl bromide

isopropylamine
75-31-0

isopropylamine

A

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

B

N-isopropyl-N,N-dibenzylamine
55578-14-8

N-isopropyl-N,N-dibenzylamine

Conditions
ConditionsYield
With sodium hydroxideA 51%
B 27%
N-isopropyl-N-ethylbenzylamine
68723-26-2

N-isopropyl-N-ethylbenzylamine

A

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

B

N-ethylbenzylamine
14321-27-8

N-ethylbenzylamine

Conditions
ConditionsYield
With iodine; sodium carbonate In chloroform at 60℃; for 24h;A 34%
B 41%
isopropylamine
75-31-0

isopropylamine

benzyl alcohol
100-51-6

benzyl alcohol

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
Pt on TiO2 for 20h; Ambient temperature; Irradiation;4.9%
benzyl bromide
100-39-0

benzyl bromide

isopropylamine
75-31-0

isopropylamine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

isopropyl phenyl ketoxime
72846-70-9, 72846-71-0, 6668-39-9

isopropyl phenyl ketoxime

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
(i) PCl5, benzene, Et2O, (ii) LiAlH4; Multistep reaction;
Diisopropoxycarbenium-tetrafluoroborat

Diisopropoxycarbenium-tetrafluoroborat

benzonitrile
100-47-0

benzonitrile

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
(i) CH2Cl2, (ii) EtOH, (iii) NaBH4; Multistep reaction;
C28H29NP(1+)*I(1-)

C28H29NP(1+)*I(1-)

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With water; hydroxide
Isopropyl-[2,2,2-trichloro-1-phenyl-eth-(E)-ylidene]-amine
76757-59-0

Isopropyl-[2,2,2-trichloro-1-phenyl-eth-(E)-ylidene]-amine

A

1-isopropyl-2-phenyl-aziridine
4164-23-2

1-isopropyl-2-phenyl-aziridine

B

N-isopropyl-(+/-)-α-methylbenzylamine
19302-16-0

N-isopropyl-(+/-)-α-methylbenzylamine

C

N-isopropyl-N-(2-phenylethyl)amine
52007-97-3

N-isopropyl-N-(2-phenylethyl)amine

D

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

E

N-(2-hydroxy-1-phenylethyl)-N-isopropylamine
68058-02-6

N-(2-hydroxy-1-phenylethyl)-N-isopropylamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether for 7h; Product distribution; Heating; various molar ratios, solvents, time. Other N-alkyl- and N-aryltrichloroacetophenone imines;A 5 % Chromat.
B 4 % Chromat.
C 64 % Chromat.
D 15 % Chromat.
E 9 % Chromat.
(E)-N-benzylidenepropan-2-amine
27845-51-8

(E)-N-benzylidenepropan-2-amine

A

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

B

(R,S)-N,N'-di(1-methylethyl)-1,2-diphenyl-1,2-ethylenediamine
55079-98-6

(R,S)-N,N'-di(1-methylethyl)-1,2-diphenyl-1,2-ethylenediamine

(R*,R*)-N,N'-di(1-methylethyl)-1,2-diphenyl-1,2-ethylenediamine

(R*,R*)-N,N'-di(1-methylethyl)-1,2-diphenyl-1,2-ethylenediamine

Conditions
ConditionsYield
With ammonium hydroxide; chloro-trimethyl-silane; water; ammonium chloride; ethylene dibromide; zinc 1.) CH3CN, 35 deg C, 1 h, 2.) CH3CN, 0 deg C; Yield given. Multistep reaction. Yields of byproduct given;
isopropyl alcohol
67-63-0

isopropyl alcohol

benzylamine
100-46-9

benzylamine

A

benzyldiisopropylamine
34636-09-4

benzyldiisopropylamine

B

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With γ-Al2O3 In gaseous matrix at 230℃; Yield given; Yields of byproduct given;
benzaldehyde isopropylimine

benzaldehyde isopropylimine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Conditions
ConditionsYield
With ethanol; nickel Hydrogenation;
phenylacetic acid
103-82-2

phenylacetic acid

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

N-benzyl-N-isopropyl-2-phenylacetamide

N-benzyl-N-isopropyl-2-phenylacetamide

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; for 14h; Inert atmosphere;100%
2,6-dichloropyridine
2402-78-0

2,6-dichloropyridine

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

2-(N-benzylisopropylamino)-6-chloropyridine
464170-02-3

2-(N-benzylisopropylamino)-6-chloropyridine

Conditions
ConditionsYield
Stage #1: Benzyl-isopropyl-amin With n-butyllithium In hexane; toluene at -64 - 0℃;
Stage #2: 2,6-dichloropyridine In hexane; toluene at 4 - 20℃;
99%
With n-butyllithium
Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

Glyoxilic acid
298-12-4

Glyoxilic acid

phenylboronic acid
98-80-6

phenylboronic acid

N-benzyl-N-isopropyl-α-phenylglycine

N-benzyl-N-isopropyl-α-phenylglycine

Conditions
ConditionsYield
In dichloromethane for 48h; Petasis reaction;99%
carbon disulfide
75-15-0

carbon disulfide

nickel(II) chloride hexahydrate

nickel(II) chloride hexahydrate

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

(benzylisopropyldithiocarbamate)2 nickel(II)
82421-76-9

(benzylisopropyldithiocarbamate)2 nickel(II)

Conditions
ConditionsYield
In ethanol; water mixing amine and CS2 in EtOH, standing for 15 min, addn. of warm H2O soln. of Ni-salt, standing for 1 h; collection (filtration), washing (warm H2O), drying (IR-lamp); elem. anal.;99%
Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

A

(Z)‑N‑isopropyl‑1‑phenylmethanimine oxide
10229-64-8, 143957-81-7, 300802-10-2

(Z)‑N‑isopropyl‑1‑phenylmethanimine oxide

B

benzaldehyde
100-52-7

benzaldehyde

Conditions
ConditionsYield
With dihydrogen peroxide; PCWP In chloroform at 40℃; for 2h;A 98%
B 2%
Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

2-Bromoacetyl bromide
598-21-0

2-Bromoacetyl bromide

N-isopropyl-N-(phenylmethyl)-2-bromoacetamide
100140-99-6

N-isopropyl-N-(phenylmethyl)-2-bromoacetamide

Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; for 1h;98%
With triethylamine In dichloromethane Ambient temperature;
With triethylamine In chloroform at 0 - 20℃; for 24h;
With triethylamine In dichloromethane at 0 - 20℃;52.2 g
tert-butyl acetoacetate
1694-31-1

tert-butyl acetoacetate

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

N-(1-methylethyl)-3-oxo-N-(phenylmethyl)butanamide

N-(1-methylethyl)-3-oxo-N-(phenylmethyl)butanamide

Conditions
ConditionsYield
at 100 - 115℃; under 100 Torr;97%
3-bromocycloheptene
36291-49-3

3-bromocycloheptene

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

(RS)-3-(N-Benzyl-N-isopropylamino)cyclohept-1-ene
1393659-10-3

(RS)-3-(N-Benzyl-N-isopropylamino)cyclohept-1-ene

Conditions
ConditionsYield
With potassium carbonate In tetrahydrofuran at 50℃; for 16h; Kinetics;96%
carbon disulfide
75-15-0

carbon disulfide

Pentafluorobenzonitrile
773-82-0

Pentafluorobenzonitrile

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

4-cyano-2,3,5,6-tetrafluorophenyl-N-benzyl-N-isopropylcarbamodithioate

4-cyano-2,3,5,6-tetrafluorophenyl-N-benzyl-N-isopropylcarbamodithioate

Conditions
ConditionsYield
Stage #1: carbon disulfide; Benzyl-isopropyl-amin With potassium phosphate In dimethyl sulfoxide at 20℃; for 2h; Schlenk technique; Green chemistry;
Stage #2: Pentafluorobenzonitrile In dimethyl sulfoxide at 20℃; for 2h; Schlenk technique; Green chemistry; regioselective reaction;
96%
Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

N-benzylideneisopropylamine N-oxide
10229-64-8, 143957-81-7, 300802-10-2

N-benzylideneisopropylamine N-oxide

Conditions
ConditionsYield
With dihydrogen peroxide; trichloroacetonitrile In methanol; water at 0 - 25℃; for 8h;95%
With sodium tungstate; dihydrogen peroxide In methanol; water at 20℃;48%
With α-D-glucose 6-phosphate; oxygen; NADP; cyclohexanone monooxygenase at 25℃; for 24h; pH=8.6; Enzymatic reaction;
With air; cyclohexanone monooxygenase from Escherichia coli; NADPH In water at 25℃; pH=8.6; Enzyme kinetics;
Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

N-benzyl-N-isopropylnitrous amide
20689-97-8

N-benzyl-N-isopropylnitrous amide

Conditions
ConditionsYield
With N,N,N’,N’-tetrabromobenzene-1,3-disulfonamide; water; silica gel; sodium nitrite In dichloromethane at 20℃; for 0.05h; Reagent/catalyst;95%
With sodium nitrite In dichloromethane at 20℃; for 0.0833333h;89%
With acetic acid; sodium nitrite In water at 0 - 20℃; for 1h; Inert atmosphere;
2-thiophenylcarboxylic acid
527-72-0

2-thiophenylcarboxylic acid

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

N-benzyl-N-isopropylthiophene-2-carboxamide

N-benzyl-N-isopropylthiophene-2-carboxamide

Conditions
ConditionsYield
Stage #1: 2-thiophenylcarboxylic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate at 20℃; for 0.166667h;
Stage #2: Benzyl-isopropyl-amin at 20℃; for 1h;
95%
styrene oxide
96-09-3

styrene oxide

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

(+/-)-benzylisopropyl(α-hydroxyphenethyl)amine
87040-39-9

(+/-)-benzylisopropyl(α-hydroxyphenethyl)amine

Conditions
ConditionsYield
In water; toluene for 3h; Heating;94%
Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

N-benzylideneisopropylamine
6852-56-8

N-benzylideneisopropylamine

Conditions
ConditionsYield
With oxygen In para-xylene at 110℃; for 1.5h;94%
With 5,10,15,20-tetrakisphenylporphyrin; oxygen In ethyl acetate at 20℃; under 760.051 Torr; for 9h; Molecular sieve; Irradiation; regioselective reaction;92%
With 5,15,10,20-tetraphenylporphyrin In acetonitrile at 30℃; for 1h; Irradiation;80%
5-methyl-imidazo[5,1-b][1,3,4]thiadiazole-2-carboxylic acid hydrochloride

5-methyl-imidazo[5,1-b][1,3,4]thiadiazole-2-carboxylic acid hydrochloride

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

5-methylimidazo[5,1-b][1,3,4]thiadiazole-2-carboxylic acid benzylisobutylamide

5-methylimidazo[5,1-b][1,3,4]thiadiazole-2-carboxylic acid benzylisobutylamide

Conditions
ConditionsYield
With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; for 2h;94%
3-methoxy-4-methyl-3-cyclobutene-1,2-dione
29769-77-5

3-methoxy-4-methyl-3-cyclobutene-1,2-dione

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

3-(benzyl(isopropyl)amino)-4-methylcyclobut-3-ene-1,2-dione

3-(benzyl(isopropyl)amino)-4-methylcyclobut-3-ene-1,2-dione

Conditions
ConditionsYield
In methanol at 20℃; for 4h;94%
Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

trifluoroacetic acid
76-05-1

trifluoroacetic acid

N-benzyl-N-(2,2,2-trifluoroethyl)propan-2-amine

N-benzyl-N-(2,2,2-trifluoroethyl)propan-2-amine

Conditions
ConditionsYield
With potassium phosphate; 18-crown-6 ether; phenylsilane In tetrahydrofuran at 80℃; for 4h; Glovebox; Molecular sieve; Schlenk technique;94%
Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

allyl bromide
106-95-6

allyl bromide

N-benzyl-N-isopropylallylamine
247033-00-7

N-benzyl-N-isopropylallylamine

Conditions
ConditionsYield
With sodium hydroxide In N,N-dimethyl-formamide for 1h; Ambient temperature;93%
Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

allyl alcohol
107-18-6

allyl alcohol

N-benzyl-N-isopropylallylamine
247033-00-7

N-benzyl-N-isopropylallylamine

Conditions
ConditionsYield
With ammonium hexafluorophosphate; [Pt(η3-C3H5)(DPP-Xantphos)]PF6 In toluene; acetonitrile at 50℃; for 8h; Inert atmosphere;93%
1-fluorodecane
334-56-5

1-fluorodecane

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

N-benzyl-N-isopropyl-1-decylamine

N-benzyl-N-isopropyl-1-decylamine

Conditions
ConditionsYield
With tris(bis(trimethylsilyl)amido)lanthanum(III) In dichloromethane at 20℃; for 7h; Inert atmosphere; chemoselective reaction;93%
2-hydroxycyclobutanone
99440-99-0

2-hydroxycyclobutanone

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

2-(benzyl(isopropyl)amino)cyclobutanone

2-(benzyl(isopropyl)amino)cyclobutanone

Conditions
ConditionsYield
With dmap In toluene at 20℃; for 15h;93%
With dmap In 1,4-dioxane at 20℃; for 1h;
Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

1,1'-carbonyldiimidazole
530-62-1

1,1'-carbonyldiimidazole

N-benzyl-N-isopropyl-1H-imidazole-1-carboxamide
55245-48-2

N-benzyl-N-isopropyl-1H-imidazole-1-carboxamide

Conditions
ConditionsYield
In tetrahydrofuran for 16h; Heating;92%
C15H13ClFN3O2

C15H13ClFN3O2

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

4-(2-fluoro-phenyl)-2-morpholin-4-yl-pyrimidine-5-carboxylic acid benzyl-isopropyl-amide

4-(2-fluoro-phenyl)-2-morpholin-4-yl-pyrimidine-5-carboxylic acid benzyl-isopropyl-amide

Conditions
ConditionsYield
In toluene at 0 - 20℃; for 1.5h;92%
methyl (RS)-5-tris(phenylthio)methylcyclopent-1-enecarboxylate
1046427-59-1

methyl (RS)-5-tris(phenylthio)methylcyclopent-1-enecarboxylate

Benzyl-isopropyl-amin
102-97-6

Benzyl-isopropyl-amin

methyl (1RS,2SR,5SR)-2-(N-benzyl-N-isopropylamino)-5-tris(phenylthio)methylcyclopentanecarboxylate

methyl (1RS,2SR,5SR)-2-(N-benzyl-N-isopropylamino)-5-tris(phenylthio)methylcyclopentanecarboxylate

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 2h;92%

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