Technology Process of C79H104O8Si4
There total 5 articles about C79H104O8Si4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 47 percent / imidazole / dimethylformamide / 5 h / 25 °C
2: 1.) ethylmagnesium bromide / 1.) Et2O, 25 degC, 30 min, benzene, 25 degC -> 80 degC; 2.) 80 degC, 20 h
3: 1.) ethylmagnesium bromide / 1.) Et2O, 25 degC, 30 min, benzene, 25 degC - 80 degC; 2.) 80 degC, 20 h
With
1H-imidazole; ethylmagnesium bromide;
In
N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)60747-5
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 47 percent / imidazole / dimethylformamide / 5 h / 25 °C
2: 1.) ethylmagnesium bromide / 1.) Et2O, 25 degC, 30 min, benzene, 25 degC -> 80 degC; 2.) 80 degC, 20 h
3: 1.) ethylmagnesium bromide / 1.) Et2O, 25 degC, 30 min, benzene, 25 degC - 80 degC; 2.) 80 degC, 20 h
With
1H-imidazole; ethylmagnesium bromide;
In
N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)60747-5
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 47 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C
2: 1.) ethylmagnesium bromide / 1.) Et2O, 25 degC, 30 min, benzene, 25 degC -> 80 degC; 2.) 80 degC, 20 h
3: 1.) ethylmagnesium bromide / 1.) Et2O, 25 degC, 30 min, benzene, 25 degC - 80 degC; 2.) 80 degC, 20 h
With
ethylmagnesium bromide; tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
DOI:10.1016/S0040-4039(00)60747-5