3-chloro-4-[(5-chloro-6-methoxypyridin-3-yl)methoxy]-N-(methylsulfonyl)benzamide

Base Information

Chemical Name:3-chloro-4-[(5-chloro-6-methoxypyridin-3-yl)methoxy]-N-(methylsulfonyl)benzamide
CAS No.:1355488-36-6
Molecular Formula:C₁₅H₁₄Cl₂N₂O₅S
Molecular Weight:405.259
Hs Code.:

Synonyms:3-chloro-4-[(5-chloro-6-methoxypyridin-3-yl)methoxy]-N-(methylsulfonyl)benzamide

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Chemical Property of 3-chloro-4-[(5-chloro-6-methoxypyridin-3-yl)methoxy]-N-(methylsulfonyl)benzamide

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Technology Process of 3-chloro-4-[(5-chloro-6-methoxypyridin-3-yl)methoxy]-N-(methylsulfonyl)benzamide

There total 4 articles about 3-chloro-4-[(5-chloro-6-methoxypyridin-3-yl)methoxy]-N-(methylsulfonyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1355489-14-3
3-chloro-4-[(5-chloro-6-methoxypyridin-3-yl)methoxy]benzamide

: 124-63-0
methanesulfonyl chloride

: 1355488-36-6
3-chloro-4-[(5-chloro-6-methoxypyridin-3-yl)methoxy]-N-(methylsulfonyl)benzamide

Guidance literature:: 3-chloro-4-[(5-chloro-6-methoxypyridin-3-yl)methoxy]benzamide; With lithium hexamethyldisilazane; In tetrahydrofuran; for 0.333333h;

methanesulfonyl chloride; In tetrahydrofuran; at 20 ℃; for 18h;

With citric acid; In tetrahydrofuran; water;

Reference yield:

: 132865-53-3
(5-chloro-6-methoxy-pyridin-3-yl)-methanol

: 1355488-36-6
3-chloro-4-[(5-chloro-6-methoxypyridin-3-yl)methoxy]-N-(methylsulfonyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

1.2: 2 h / 20 °C

2.1: dihydrogen peroxide; potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.33 h

3.2: 18 h / 20 °C

With dihydrogen peroxide; sodium hydride; potassium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 117482-84-5
3-chloro-4-fluorobenzonitrile

: 1355488-36-6
3-chloro-4-[(5-chloro-6-methoxypyridin-3-yl)methoxy]-N-(methylsulfonyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

1.2: 2 h / 20 °C

2.1: dihydrogen peroxide; potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.33 h

3.2: 18 h / 20 °C

With dihydrogen peroxide; sodium hydride; potassium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;