O-[7-azido-1-(phenylsulfonyl)-2-heptyl]-N-[4’-(diethylcarbamoyl)phenyl]carbamate

Base Information

Chemical Name:O-[7-azido-1-(phenylsulfonyl)-2-heptyl]-N-[4’-(diethylcarbamoyl)phenyl]carbamate
CAS No.:1346434-56-7
Molecular Formula:C₂₅H₃₃N₅O₅S
Molecular Weight:515.634
Hs Code.:

Synonyms:O-[7-azido-1-(phenylsulfonyl)-2-heptyl]-N-[4’-(diethylcarbamoyl)phenyl]carbamate

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Chemical Property of O-[7-azido-1-(phenylsulfonyl)-2-heptyl]-N-[4’-(diethylcarbamoyl)phenyl]carbamate

Chemical Property:

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Technology Process of O-[7-azido-1-(phenylsulfonyl)-2-heptyl]-N-[4’-(diethylcarbamoyl)phenyl]carbamate

There total 8 articles about O-[7-azido-1-(phenylsulfonyl)-2-heptyl]-N-[4’-(diethylcarbamoyl)phenyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1346434-36-3
1-(phenylsulfonyl)-7-azido-2-heptyl chloroformate

: 51207-85-3
4-amino-N,N-diethylbenzamide

: 1346434-56-7
O-[7-azido-1-(phenylsulfonyl)-2-heptyl]-N-[4’-(diethylcarbamoyl)phenyl]carbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; for 1h;

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 1346434-56-7
O-[7-azido-1-(phenylsulfonyl)-2-heptyl]-N-[4’-(diethylcarbamoyl)phenyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 1 h / Cooling with ice

2: ammonium formate / palladium 10% on activated carbon / methanol / 2 h / 20 °C

3: triethylamine / tetrahydrofuran / 1 h

With ammonium formate; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 5323-47-7
N,N-diethyl-4-nitrobenzamide

: 1346434-56-7
O-[7-azido-1-(phenylsulfonyl)-2-heptyl]-N-[4’-(diethylcarbamoyl)phenyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium formate / palladium 10% on activated carbon / methanol / 2 h / 20 °C

2: triethylamine / tetrahydrofuran / 1 h

With ammonium formate; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol;