O-[1-(phenylsulfonyl)-7-azido-2-heptyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethyl carbamate

Base Information

Chemical Name:O-[1-(phenylsulfonyl)-7-azido-2-heptyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethyl carbamate
CAS No.:1346434-61-4
Molecular Formula:C₂₆H₃₄ClN₅O₅S
Molecular Weight:564.105
Hs Code.:

Synonyms:O-[1-(phenylsulfonyl)-7-azido-2-heptyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethyl carbamate

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Chemical Property of O-[1-(phenylsulfonyl)-7-azido-2-heptyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethyl carbamate

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Technology Process of O-[1-(phenylsulfonyl)-7-azido-2-heptyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethyl carbamate

There total 10 articles about O-[1-(phenylsulfonyl)-7-azido-2-heptyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1346434-56-7
O-[7-azido-1-(phenylsulfonyl)-2-heptyl]-N-[4’-(diethylcarbamoyl)phenyl]carbamate

: 1346434-61-4
O-[1-(phenylsulfonyl)-7-azido-2-heptyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethyl carbamate

Guidance literature:: With chloro-trimethyl-silane; triethylamine; In tetrahydrofuran; at 55 ℃; for 17h;

Reference yield:

: 5323-47-7
N,N-diethyl-4-nitrobenzamide

: 1346434-61-4
O-[1-(phenylsulfonyl)-7-azido-2-heptyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethyl carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium formate / palladium 10% on activated carbon / methanol / 2 h / 20 °C

2: triethylamine / tetrahydrofuran / 1 h

3: chloro-trimethyl-silane; triethylamine / tetrahydrofuran / 17 h / 55 °C

With chloro-trimethyl-silane; ammonium formate; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol;

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 1346434-61-4
O-[1-(phenylsulfonyl)-7-azido-2-heptyl]-N-[4-(diethylcarboxamido)phenyl]-N-chloromethyl carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 1 h / Cooling with ice

2: ammonium formate / palladium 10% on activated carbon / methanol / 2 h / 20 °C

3: triethylamine / tetrahydrofuran / 1 h

4: chloro-trimethyl-silane; triethylamine / tetrahydrofuran / 17 h / 55 °C

With chloro-trimethyl-silane; ammonium formate; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane;