Malonic acid tert-butyl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Base Information

Chemical Name:Malonic acid tert-butyl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester
CAS No.:67406-69-3
Molecular Formula:C₁₇H₃₀O₄
Molecular Weight:298.423
Hs Code.:

Synonyms:Malonic acid tert-butyl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Malonic acid tert-butyl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Chemical Property:

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Technology Process of Malonic acid tert-butyl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

There total 1 articles about Malonic acid tert-butyl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40052-13-9
mono-tert-butyl malonate

: 2216-51-5
(-)-menthol

: 67406-69-3
Malonic acid tert-butyl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.tetlet.2005.05.044

Reference yield:

: 67406-69-3
Malonic acid tert-butyl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 53943-72-9
3-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-3-oxopropanoic acid

Guidance literature:: With triethylamine tris(hydrogen fluoride); In dichloromethane;
DOI:10.1016/j.tetlet.2005.05.044

Reference yield:

: 67406-69-3
Malonic acid tert-butyl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: Malonic acid 4-hydroxy-benzyl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N*3HF / CH₂Cl₂

2: DCC / CH₂Cl₂

With triethylamine tris(hydrogen fluoride); dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.tetlet.2005.05.044