methyl 2-(tert-butoxy)-2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate

Base Information

Chemical Name:methyl 2-(tert-butoxy)-2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate
CAS No.:1428794-64-2
Molecular Formula:C₂₃H₂₈N₂O₄
Molecular Weight:396.486
Hs Code.:

Synonyms:methyl 2-(tert-butoxy)-2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate

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Chemical Property of methyl 2-(tert-butoxy)-2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate

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Technology Process of methyl 2-(tert-butoxy)-2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate

There total 3 articles about methyl 2-(tert-butoxy)-2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.4%

: 540-88-5
acetic acid tert-butyl ester

: 1428794-63-1
methyl 2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridine-5-yl)-2-hydroxyacetate

: 1428794-64-2
methyl 2-(tert-butoxy)-2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate

Guidance literature:: With perchloric acid; for 48h; Cooling with ice;

Reference yield:

: 1428794-60-8
methyl 2-hydroxy-2-(1-(4-methoxybenzyl)-6-methyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate

: 1428794-64-2
methyl 2-(tert-butoxy)-2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; trifluoroacetic acid; methoxybenzene / 3 h / 20 °C / Cooling with ice

2: caesium carbonate / 6 h / 50 °C

3: perchloric acid / 48 h / Cooling with ice

With perchloric acid; sulfuric acid; caesium carbonate; methoxybenzene; trifluoroacetic acid;

Reference yield:

: 1428794-61-9
methyl 2-hydroxy-2-(6-methyl-7-oxo-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate

: 1428794-64-2
methyl 2-(tert-butoxy)-2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / 6 h / 50 °C

2: perchloric acid / 48 h / Cooling with ice

With perchloric acid; caesium carbonate;