methyl 2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridine-5-yl)-2-hydroxyacetate

Base Information

Chemical Name:methyl 2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridine-5-yl)-2-hydroxyacetate
CAS No.:1428794-63-1
Molecular Formula:C₁₉H₂₀N₂O₄
Molecular Weight:340.379
Hs Code.:

Synonyms:methyl 2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridine-5-yl)-2-hydroxyacetate

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Chemical Property of methyl 2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridine-5-yl)-2-hydroxyacetate

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Technology Process of methyl 2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridine-5-yl)-2-hydroxyacetate

There total 2 articles about methyl 2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridine-5-yl)-2-hydroxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.6%

: 1428794-61-9
methyl 2-hydroxy-2-(6-methyl-7-oxo-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate

: 74-88-4
methyl iodide

: 1428794-63-1
methyl 2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridine-5-yl)-2-hydroxyacetate

Guidance literature:: With caesium carbonate; at 50 ℃; for 6h;

Reference yield:

: 1428794-60-8
methyl 2-hydroxy-2-(1-(4-methoxybenzyl)-6-methyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridin-5-yl)acetate

: 1428794-63-1
methyl 2-(1,6-dimethyl-7-oxo-4-(p-tolyl)-6,7-dihydro-1H-pyrrolo[2,3-c]pyridine-5-yl)-2-hydroxyacetate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; trifluoroacetic acid; methoxybenzene / 3 h / 20 °C / Cooling with ice

2: caesium carbonate / 6 h / 50 °C

With sulfuric acid; caesium carbonate; methoxybenzene; trifluoroacetic acid;