(Z)-methyl N-3-chloro-4-(phenylsulfonyl)phenyl-N'-cyanocarbamimidothioate

Base Information

Chemical Name:(Z)-methyl N-3-chloro-4-(phenylsulfonyl)phenyl-N'-cyanocarbamimidothioate
CAS No.:1620878-62-7
Molecular Formula:C₁₅H₁₂ClN₃O₂S₂
Molecular Weight:365.864
Hs Code.:

Synonyms:(Z)-methyl N-3-chloro-4-(phenylsulfonyl)phenyl-N'-cyanocarbamimidothioate

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Chemical Property of (Z)-methyl N-3-chloro-4-(phenylsulfonyl)phenyl-N'-cyanocarbamimidothioate

Chemical Property:

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Technology Process of (Z)-methyl N-3-chloro-4-(phenylsulfonyl)phenyl-N'-cyanocarbamimidothioate

There total 6 articles about (Z)-methyl N-3-chloro-4-(phenylsulfonyl)phenyl-N'-cyanocarbamimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.3%

: 1620783-08-5
2-chloro-4-isothiocyanato-1-(phenylsulfonyl)benzene

: 19981-17-0,20611-81-8,123092-13-7,17292-62-5
sodium cyanamide

: 74-88-4
methyl iodide

: 1620878-62-7
(Z)-methyl N-3-chloro-4-(phenylsulfonyl)phenyl-N'-cyanocarbamimidothioate

Guidance literature:: sodium cyanamide; With sodium methylate; In methanol; for 0.25h;

2-chloro-4-isothiocyanato-1-(phenylsulfonyl)benzene; In methanol; at 20 ℃; for 1h;

methyl iodide; In methanol; at 20 ℃;

Reference yield:

: 29482-57-3
2-chloro-4-nitro-1-phenylsulfanylbenzene

: 1620878-62-7
(Z)-methyl N-3-chloro-4-(phenylsulfonyl)phenyl-N'-cyanocarbamimidothioate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Cooling with ice

2.1: iron; ammonium chloride / water; methanol / 6 h / Reflux

3.1: calcium carbonate / water; dichloromethane / 0.17 h / 0 °C / Inert atmosphere

3.2: 4 h / 0 - 20 °C / Inert atmosphere

4.1: sodium methylate / methanol / 0.25 h

4.2: 1 h / 20 °C

4.3: 20 °C

With sodium methylate; iron; ammonium chloride; 3-chloro-benzenecarboperoxoic acid; calcium carbonate; In methanol; dichloromethane; water;

Reference yield:

: 32631-24-6
(2-chloro-4-nitrophenyl)(phenyl)sulfone

: 1620878-62-7
(Z)-methyl N-3-chloro-4-(phenylsulfonyl)phenyl-N'-cyanocarbamimidothioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: iron; ammonium chloride / water; methanol / 6 h / Reflux

2.1: calcium carbonate / water; dichloromethane / 0.17 h / 0 °C / Inert atmosphere

2.2: 4 h / 0 - 20 °C / Inert atmosphere

3.1: sodium methylate / methanol / 0.25 h

3.2: 1 h / 20 °C

3.3: 20 °C

With sodium methylate; iron; ammonium chloride; calcium carbonate; In methanol; dichloromethane; water;