Technology Process of 3-[3-(2-Ethoxycarbonyl-ethyl)-4-hexyloxy-benzoyl]-benzoic acid ethyl ester
There total 6 articles about 3-[3-(2-Ethoxycarbonyl-ethyl)-4-hexyloxy-benzoyl]-benzoic acid ethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine (TEA) / diethyl ether
2: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C
With
sodium hydride; triethylamine;
In
diethyl ether;
DOI:10.1021/jm00172a020
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) AlCl3 / 1.) CH2Cl2, 0 deg C, 1 h, 2.) 0 deg C, 4 h
2: 92 percent / pyridine hydrochloride / 4 h / 180 °C
3: 56 percent / sulfuric acid / 96 h / Heating
4: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C
With
aluminium trichloride; sulfuric acid; pyridine hydrochloride; sodium hydride;
DOI:10.1021/jm00172a020
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) AlCl3 / 1.) CH2Cl2, 0 deg C, 1 h, 2.) 0 deg C, 4 h
2: 92 percent / pyridine hydrochloride / 4 h / 180 °C
3: 56 percent / sulfuric acid / 96 h / Heating
4: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C
With
aluminium trichloride; sulfuric acid; pyridine hydrochloride; sodium hydride;
DOI:10.1021/jm00172a020
