N,N'-bis(2,3,4-trimethoxybenzylidene)-1,2-diaminoethane

Base Information

Chemical Name:N,N'-bis(2,3,4-trimethoxybenzylidene)-1,2-diaminoethane
CAS No.:67175-92-2
Molecular Formula:C₂₂H₂₈N₂O₆
Molecular Weight:416.474
Hs Code.:

Synonyms:N,N'-bis(2,3,4-trimethoxybenzylidene)-1,2-diaminoethane

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Chemical Property of N,N'-bis(2,3,4-trimethoxybenzylidene)-1,2-diaminoethane

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Technology Process of N,N'-bis(2,3,4-trimethoxybenzylidene)-1,2-diaminoethane

There total 1 articles about N,N'-bis(2,3,4-trimethoxybenzylidene)-1,2-diaminoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 107-15-3,85404-18-8
ethylenediamine

: 2103-57-3
2,3,4-trimethoxybenzaldehyde

: 67175-92-2
N,N'-bis(2,3,4-trimethoxybenzylidene)-1,2-diaminoethane

Guidance literature:: In methanol; at 50 ℃;
DOI:10.1134/S1070328411080045

Reference yield: 83.0%

: 67175-92-2
N,N'-bis(2,3,4-trimethoxybenzylidene)-1,2-diaminoethane

: 10139-47-6
zinc(II) iodide

: [ZnI₂(N,N'-bis(2,3,4-trimethoxybenzylidene)-1,2-diaminoethane)]

Guidance literature:: In methanol; chloroform; soln. of ZnI2 in MeOH added to soln. of Schiff base in CHCl3 under stirring, mixt. (molar ratio = 1:1) stirred at room temp. for 10 min; crystn. at 0°C for several d, crystals filtered off, washed with Et2O; elem. anal.;
DOI:10.1134/S1070328411080045

Reference yield: 75.0%

: 67175-92-2
N,N'-bis(2,3,4-trimethoxybenzylidene)-1,2-diaminoethane

: mercury dichloride

: 1333081-63-2
[HgCl₂(N,N'-bis(2,3,4-trimethoxybenzylidene)-1,2-diaminoethane)]

Guidance literature:: In methanol; acetonitrile; soln. of ZnI2 in MeOH added to soln. of Schiff base in MeCN under stirring, mixt. (molar ratio = 1:1) stirred at room temp. for 0.5 h; evapn. at 40°C under vac., residue dissolved in CHCl3, crystn. at0°C for several d, solid filtered off, washed with Et2O; elem. a nal.;
DOI:10.1134/S1070328411080045