ReH₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

Base Information

Chemical Name:ReH₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2
CAS No.:17300-50-4
Molecular Formula:C₅₂H₅₁P₄Re
Molecular Weight:986.079
Hs Code.:

ReH<sub>3</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2

Synonyms:ReH₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

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Chemical Property of ReH₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

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Technology Process of ReH₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

There total 2 articles about ReH₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 79245-21-9,92077-24-2
ReH₅(PMePh₂)₃

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 17300-50-4
ReH₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

Guidance literature:: mixture of starting materials is heated in a Schlenk flask at 180 - 200°C under vac. for 2 h in the absence of solvents; cooling to room temp., addn. of EtOH, stirring overnight, filtn., washing with EtOH and acetone, vac. drying;

Reference yield:

: Re((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2(CHO₂)

: 17300-50-4
ReH₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

Guidance literature:: With hydrogen; In benzene; storage of benzene soln. of complex under H2;

Reference yield: 70.0%

: 17300-50-4
ReH₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 29663-54-5
tropylium hexafluorophosphate

: 108530-69-4
ReH₂((C₆H₅)2PC₂H₄P(C₆H₅)2)2(CNC₄H₉)⁽¹⁺⁾*PF₆^(1-)={ReH₂((C₆H₅)2PC₂H₄P(C₆H₅)2)2(CNC₄H₉)}PF₆

Guidance literature:: In dichloromethane; CH2Cl2, a three-fold excess of t-BuNC, N2 atm.;; Et2O and pentane was added, ppt. was filtered off and dried; elem. anal.;;
DOI:10.1039/DT9870000715