C₃₀H₅₁N₃O₁₃S₄

Base Information

• Chemical Name: C₃₀H₅₁N₃O₁₃S₄
• CAS No.: 1415712-87-6
• Molecular Formula: C₃₀H₅₁N₃O₁₃S₄
• Molecular Weight: 790.011

Synonyms:C₃₀H₅₁N₃O₁₃S₄

Chemical Property of C₃₀H₅₁N₃O₁₃S₄

Chemical Property:

Purity/Quality:

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Technology Process of C₃₀H₅₁N₃O₁₃S₄

There total 1 articles about C₃₀H₅₁N₃O₁₃S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-(2-aminoethoxy)ethoxy)ethan-1-ol (6338-55-2) → C30H51N3O13S4 (1415712-87-6)

Guidance literature:

Multi-step reaction with 7 steps

1.1: sodium hydrogencarbonate / water; acetonitrile / 2 h / 0 - 20 °C / Inert atmosphere

2.1: potassium hydrogencarbonate / acetonitrile / 72 h / 80 °C / Inert atmosphere

3.1: sodium iodide / acetone / 20 h / 20 °C / Inert atmosphere

3.2: polymer-supported triphenylphosphine / 1.67 h / 0 - 20 °C / Inert atmosphere

3.3: 4.17 h / 0 - 20 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

4.2: 0.83 h / 0 - 20 °C / Inert atmosphere

5.1: potassium permanganate / water; acetic acid / 1 h / -15 - -10 °C / Inert atmosphere

6.1: palladium on activated charcoal; hydrogen / ethanol; ethyl acetate / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

7.1: N-ethylmorpholine; / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

With N-ethylmorpholine;; potassium permanganate; palladium on activated charcoal; hydrogen; sodium hydrogencarbonate; potassium hydrogencarbonate; triethylamine; sodium iodide; In ethanol; dichloromethane; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide; acetone; acetonitrile; 2.1: |Michael Addition;

DOI:10.1016/j.tet.2011.10.100

upstream raw materials:

2-(2-(2-aminoethoxy)ethoxy)ethan-1-ol

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