N-Phenyl-N'-[(E)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-prop-2-en-(E)-ylidene]-hydrazine

Base Information

• Chemical Name: N-Phenyl-N'-[(E)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-prop-2-en-(E)-ylidene]-hydrazine
• CAS No.: 314045-13-1
• Molecular Formula: C₁₅H₂₁BN₂O₂
• Molecular Weight: 272.155

Synonyms:N-Phenyl-N'-[(E)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-prop-2-en-(E)-ylidene]-hydrazine

Chemical Property of N-Phenyl-N'-[(E)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-prop-2-en-(E)-ylidene]-hydrazine

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Technology Process of N-Phenyl-N'-[(E)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-prop-2-en-(E)-ylidene]-hydrazine

There total 3 articles about N-Phenyl-N'-[(E)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-prop-2-en-(E)-ylidene]-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylhydrazine (100-63-0) + (2E)-3-(4,4,5,5-tetramethyl-1,2,3-dioxaborolan-2-yl)prop-2-enal (153725-01-0) → N-Phenyl-N'-[(E)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-prop-2-en-(E)-ylidene]-hydrazine (314045-13-1)

Guidance literature:

With disodium hydrogenphosphate; In diethyl ether; water; at 50 ℃; for 0.5h;

DOI:10.1021/ol006626b

Reference yield:

2,3-dimethyl-2,3-butane diol (76-09-5) → N-Phenyl-N'-[(E)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-prop-2-en-(E)-ylidene]-hydrazine (314045-13-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / tetrahydrofuran / 0.5 h / 20 °C

2: MgSO₄ / CH₂Cl₂ / 2 h / Heating

With magnesium sulfate; In tetrahydrofuran; dichloromethane;

DOI:10.1002/chem.200390049

Reference yield:

phenylhydrazine (100-63-0) + (2E)-3-(4,4,5,5-tetramethyl-1,2,3-dioxaborolan-2-yl)prop-2-enal (153725-01-0) → N-Phenyl-N'-[(E)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-prop-2-en-(Z)-ylidene]-hydrazine + N-Phenyl-N'-[(E)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-prop-2-en-(E)-ylidene]-hydrazine (314045-13-1)

Guidance literature:

With magnesium sulfate; In dichloromethane; for 2h; Title compound not separated from byproducts.; Heating;

DOI:10.1002/chem.200390049

upstream raw materials:

phenylhydrazine

(2E)-3-(4,4,5,5-tetramethyl-1,2,3-dioxaborolan-2-yl)prop-2-enal

2,3-dimethyl-2,3-butane diol

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