Dodecyl-phosphonic acid methyl ester (1S,3R,4S,5S,6R)-3,4,5,6-tetrakis-benzyloxy-2,2-difluoro-cyclohexyl ester

Base Information

Chemical Name:Dodecyl-phosphonic acid methyl ester (1S,3R,4S,5S,6R)-3,4,5,6-tetrakis-benzyloxy-2,2-difluoro-cyclohexyl ester
CAS No.:172607-66-8
Molecular Formula:C₄₇H₆₁F₂O₇P
Molecular Weight:806.968
Hs Code.:

Synonyms:Dodecyl-phosphonic acid methyl ester (1S,3R,4S,5S,6R)-3,4,5,6-tetrakis-benzyloxy-2,2-difluoro-cyclohexyl ester

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Chemical Property of Dodecyl-phosphonic acid methyl ester (1S,3R,4S,5S,6R)-3,4,5,6-tetrakis-benzyloxy-2,2-difluoro-cyclohexyl ester

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Technology Process of Dodecyl-phosphonic acid methyl ester (1S,3R,4S,5S,6R)-3,4,5,6-tetrakis-benzyloxy-2,2-difluoro-cyclohexyl ester

There total 5 articles about Dodecyl-phosphonic acid methyl ester (1S,3R,4S,5S,6R)-3,4,5,6-tetrakis-benzyloxy-2,2-difluoro-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 67-56-1
methanol

: 3586-98-9
n-dodecylphosphonic acid dichloride

: (1S,3R,4S,5R,6S)-3,4,5,6-Tetrakis-benzyloxy-2,2-difluoro-cyclohexanol

: 172607-66-8
Dodecyl-phosphonic acid methyl ester (1S,3R,4S,5S,6R)-3,4,5,6-tetrakis-benzyloxy-2,2-difluoro-cyclohexyl ester

Guidance literature:: With base; at 0 ℃;
DOI:10.1016/0040-4039(95)01579-5

Reference yield:

: 172722-79-1
1-O-benzoyl-3,4,5,6-tetra-O-benzyl-myo-inositol

: 172607-66-8
Dodecyl-phosphonic acid methyl ester (1S,3R,4S,5S,6R)-3,4,5,6-tetrakis-benzyloxy-2,2-difluoro-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / Ac₂O / dimethylsulfoxide

2: 62 percent / DAST / CH₂Cl₂ / 0 °C

3: 91 percent / NaOH / H₂O / Ambient temperature

4: 65 percent / base / 0 °C

With sodium hydroxide; acetic anhydride; 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/0040-4039(95)01579-5

Reference yield:

: 24558-77-8
3,4,5,6-tetra-O-benzyl inositol

: 172607-66-8
Dodecyl-phosphonic acid methyl ester (1S,3R,4S,5S,6R)-3,4,5,6-tetrakis-benzyloxy-2,2-difluoro-cyclohexyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / base

2: 88 percent / Ac₂O / dimethylsulfoxide

3: 62 percent / DAST / CH₂Cl₂ / 0 °C

4: 91 percent / NaOH / H₂O / Ambient temperature

5: 65 percent / base / 0 °C

With sodium hydroxide; acetic anhydride; 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/0040-4039(95)01579-5