4,4'-oxybistrimethylsilane

Base Information

Chemical Name:4,4'-oxybistrimethylsilane
CAS No.:112474-71-2
Molecular Formula:C₃₂H₃₆Cl₂OS₂Si₂
Molecular Weight:627.846
Hs Code.:

4,4'-oxybis<phenyl(4-chlorophenylthio)methyl>trimethylsilane

Synonyms:4,4'-oxybistrimethylsilane

Suppliers and Price of 4,4'-oxybistrimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-oxybistrimethylsilane

Chemical Property:

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Technology Process of 4,4'-oxybistrimethylsilane

There total 3 articles about 4,4'-oxybistrimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 101-84-8
diphenylether

: 103559-17-7
trimethylsilane

: 112474-62-1
<4-chlorophenylthio(4-phenoxyphenyl)methyl>trimethylsilane

: 112474-71-2
4,4'-oxybistrimethylsilane

Guidance literature:: tin(IV) chloride; In dichloromethane; at -20 ℃; for 0.5h;

Reference yield:

: 112474-70-1
<(4-chlorophenylthio)methyl>trimethylsilane

: 112474-71-2
4,4'-oxybistrimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / N-chlorosuccinimide / CCl₄ / 15 h / Ambient temperature

2: 30 percent / SnCl₄ / CH₂Cl₂ / 0.5 h / -20 °C / molar ratio 1f:2:SnCl₄=1:3:4.5

With N-chloro-succinimide; tin(IV) chloride; In tetrachloromethane; dichloromethane;

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 112474-71-2
4,4'-oxybistrimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / NaOH / H₂O; ethanol / 4 h / Heating

2: 90 percent / N-chlorosuccinimide / CCl₄ / 15 h / Ambient temperature

3: 30 percent / SnCl₄ / CH₂Cl₂ / 0.5 h / -20 °C / molar ratio 1f:2:SnCl₄=1:3:4.5

With sodium hydroxide; N-chloro-succinimide; tin(IV) chloride; In tetrachloromethane; ethanol; dichloromethane; water;