3-[(4-Nitrophenyl)azo]-9H-carbazole-9-ethanol

Base Information

Chemical Name:3-[(4-Nitrophenyl)azo]-9H-carbazole-9-ethanol
CAS No.:177100-04-8
Molecular Formula:C₂₀H₁₆N₄O₃
Molecular Weight:360.372
Hs Code.:
European Community (EC) Number:621-148-8
DSSTox Substance ID:DTXSID301040486
Nikkaji Number:J2.754.822I
Mol file:177100-04-8.mol

Synonyms:177100-04-8;3-[(4-Nitrophenyl)azo]-9H-carbazole-9-ethanol;2-[3-[(4-nitrophenyl)diazenyl]carbazol-9-yl]ethanol;2-(3-((4-Nitrophenyl)diazenyl)-9h-carbazol-9-yl)ethan-1-ol;SCHEMBL690701;SCHEMBL10068853;DTXSID301040486;3-((4-Nitrophenyl)azo)-9H-carbazole-;3-(4-Nitrophenylazo)-9H-carbazole-9-ethanol;9H-Carbazole-9-ethanol, 3-[2-(4-nitrophenyl)diazenyl]-

Suppliers and Price of 3-[(4-Nitrophenyl)azo]-9H-carbazole-9-ethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
3-[(4-NITROPHENYL)AZO]-9H-CARBAZOLE-9-ETHANOL Aldrich
10mg
$ 111.00

Total 2 raw suppliers

Chemical Property of 3-[(4-Nitrophenyl)azo]-9H-carbazole-9-ethanol

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:360.12224039
Heavy Atom Count:27
Complexity:544

Purity/Quality:

98%+ ^*data from raw suppliers

3-[(4-NITROPHENYL)AZO]-9H-CARBAZOLE-9-ETHANOL Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=C(N2CCO)C=CC(=C3)N=NC4=CC=C(C=C4)[N+](=O)[O-]

Technology Process of 3-[(4-Nitrophenyl)azo]-9H-carbazole-9-ethanol

There total 2 articles about 3-[(4-Nitrophenyl)azo]-9H-carbazole-9-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1484-14-6
2-carbazol-9-yl-ethanol

: 100-01-6,104810-17-5
4-nitro-aniline

: 177100-04-8
3-[(4-nitrophenyl)]azo-9H-carbazole-9-ethanol

Guidance literature:: 4-nitro-aniline; With hydrogenchloride; sodium dodecyl-sulfate; sodium nitrite; In water; at 0 ℃;

2-carbazol-9-yl-ethanol; In dichloromethane; water; at 20 ℃; for 24h;
DOI:10.1016/j.polymer.2016.06.042

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 177100-04-8
3-[(4-nitrophenyl)]azo-9H-carbazole-9-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / N,N-dimethyl-formamide / 20 °C

2: sodium nitrite; hydrogenchloride / water / 0 °C

With hydrogenchloride; potassium hydroxide; sodium nitrite; In water; N,N-dimethyl-formamide;
DOI:10.1021/acs.macromol.5b02401