benzyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-5-O-mesyl-β-D-glucofuranoside

Base Information

Chemical Name:benzyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-5-O-mesyl-β-D-glucofuranoside
CAS No.:79943-12-7
Molecular Formula:C₃₀H₃₁NO₁₀S
Molecular Weight:597.643
Hs Code.:

Synonyms:benzyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-5-O-mesyl-β-D-glucofuranoside

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Chemical Property of benzyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-5-O-mesyl-β-D-glucofuranoside

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Technology Process of benzyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-5-O-mesyl-β-D-glucofuranoside

There total 5 articles about benzyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-5-O-mesyl-β-D-glucofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 124-63-0
methanesulfonyl chloride

: 79943-11-6
benzyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-glucofuranoside

: 79943-12-7
benzyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-5-O-mesyl-β-D-glucofuranoside

Guidance literature:: With pyridine; for 4h; Ambient temperature;
DOI:10.1016/S0008-6215(00)80713-2

Reference yield:

: 58886-33-2
benzyl 2-acetamido-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

: 79943-12-7
benzyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-5-O-mesyl-β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 1.5 h / 0 °C

2: 90 percent / acetic acid / H₂O / 1.5 h / 50 °C

3: 84 percent / pyridine / 5 h / -10 °C

4: 91 percent / pyridine / 4 h / Ambient temperature

With pyridine; acetic acid; In water;
DOI:10.1016/S0008-6215(00)80713-2

Reference yield:

: 98-88-4
benzoyl chloride

: 79943-12-7
benzyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-5-O-mesyl-β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 1.5 h / 0 °C

2: 90 percent / acetic acid / H₂O / 1.5 h / 50 °C

3: 84 percent / pyridine / 5 h / -10 °C

4: 91 percent / pyridine / 4 h / Ambient temperature

With pyridine; acetic acid; In water;
DOI:10.1016/S0008-6215(00)80713-2