PCl(mesityl)CHPh₂

Base Information

Chemical Name:PCl(mesityl)CHPh₂
CAS No.:67565-90-6
Molecular Formula:C₂₂H₂₂ClP
Molecular Weight:352.843
Hs Code.:

Synonyms:PCl(mesityl)CHPh₂

Suppliers and Price of PCl(mesityl)CHPh₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of PCl(mesityl)CHPh₂

Chemical Property:

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Technology Process of PCl(mesityl)CHPh₂

There total 6 articles about PCl(mesityl)CHPh₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67565-91-7
mesityldiphenylmethylenephoshine

: 67565-90-6
PCl(mesityl)CHPh₂

Guidance literature:: With hydrogenchloride;
DOI:10.1021/ja00483a041

Reference yield:

: 576-83-0
2,4,6-trimethylphenyl bromide

: 67565-90-6
PCl(mesityl)CHPh₂

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Mg / 1.) THF, 2.) THF, -40 deg C to -50 deg C, 1.5h

2: 49 percent / 1.68N HCl / diethyl ether

3: 1.) 1.5N n-butyllithium / 1.) THF, hexane, 2.) 20h, RT

4: 73 percent Spectr_. / 2.14N HCl / tetrahydrofuran; diethyl ether

With hydrogenchloride; n-butyllithium; magnesium; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4020(01)91106-8