(4-perfluorohexylsulfanyl-phenyl)-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:(4-perfluorohexylsulfanyl-phenyl)-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside
CAS No.:551935-38-7
Molecular Formula:C₂₆H₂₃F₁₃O₁₀S
Molecular Weight:774.508
Hs Code.:

Synonyms:(4-perfluorohexylsulfanyl-phenyl)-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-perfluorohexylsulfanyl-phenyl)-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of (4-perfluorohexylsulfanyl-phenyl)-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

There total 3 articles about (4-perfluorohexylsulfanyl-phenyl)-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 551935-36-5
4-(perfluorohexylsulfanyl)-phenol

: 604-69-3
β-D-glucose pentaacetate

: 551935-38-7
(4-perfluorohexylsulfanyl-phenyl)-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In diethyl ether; dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/S0022-1139(02)00310-X

Reference yield:

: 355-43-1
n-perfluorohexyl iodide

: 551935-38-7
(4-perfluorohexylsulfanyl-phenyl)-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / aq. NaHCO₃; Na₂S₂O₄ / dimethylformamide / 1.5 h / 0 - 20 °C

2: 66 percent / BF₃*Et₂O / CH₂Cl₂; diethyl ether / 24 h / 20 °C

With sodium dithionite; boron trifluoride diethyl etherate; sodium hydrogencarbonate; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0022-1139(02)00310-X

Reference yield:

: 637-89-8
4-sulfanylphenol

: 551935-38-7
(4-perfluorohexylsulfanyl-phenyl)-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / aq. NaHCO₃; Na₂S₂O₄ / dimethylformamide / 1.5 h / 0 - 20 °C

2: 66 percent / BF₃*Et₂O / CH₂Cl₂; diethyl ether / 24 h / 20 °C

With sodium dithionite; boron trifluoride diethyl etherate; sodium hydrogencarbonate; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0022-1139(02)00310-X