N-[(diethylamino)carbonyl]-2,3:4,5-bis-O-(1-methylethylidene)-β-D-fructopyranose sulfamate

Base Information

Chemical Name:N-[(diethylamino)carbonyl]-2,3:4,5-bis-O-(1-methylethylidene)-β-D-fructopyranose sulfamate
CAS No.:876403-98-4
Molecular Formula:C₁₇H₃₀N₂O₉S
Molecular Weight:438.499
Hs Code.:

Synonyms:N-[(diethylamino)carbonyl]-2,3:4,5-bis-O-(1-methylethylidene)-β-D-fructopyranose sulfamate

Suppliers and Price of N-[(diethylamino)carbonyl]-2,3:4,5-bis-O-(1-methylethylidene)-β-D-fructopyranose sulfamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,3:4,5-Bis-O-(1-methylethylidene)-β-D-fructopyranose1-[[(diethylamino)carbonyl]sulfamate]
1g
$ 1165.00

TRC
2,3:4,5-Bis-O-(1-methylethylidene)-β-D-fructopyranose1-[[(diethylamino)carbonyl]sulfamate]
500mg
$ 605.00

Total 5 raw suppliers

Chemical Property of N-[(diethylamino)carbonyl]-2,3:4,5-bis-O-(1-methylethylidene)-β-D-fructopyranose sulfamate

Chemical Property:

Melting Point:110 - 112°C
Density:1.267±0.06 g/cm3(Predicted)

Purity/Quality:

95% min ^*data from raw suppliers

2,3:4,5-Bis-O-(1-methylethylidene)-β-D-fructopyranose1-[[(diethylamino)carbonyl]sulfamate] ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 2,3:4,5-Bis-O-(1-methylethylidene)-β-D-fructopyranose 1-[[(diethylamino)carbonyl]sulfamate] is an impurity of Topiramate (T540250), which is used as an anti-convulsant.

Technology Process of N-[(diethylamino)carbonyl]-2,3:4,5-bis-O-(1-methylethylidene)-β-D-fructopyranose sulfamate

There total 3 articles about N-[(diethylamino)carbonyl]-2,3:4,5-bis-O-(1-methylethylidene)-β-D-fructopyranose sulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.4%

: 876403-98-4
N-[(diethylamino)carbonyl]-2,3:4,5-bis-O-(1-methylethylidene)-β-D-fructopyranose sulfamate

Guidance literature:: Purification / work up;

Reference yield: 54.0%

: 20880-92-6
2,3;4,5-di-O-isopropylidene-β-D-fructopyranose

: 1189-71-5
isocyanate de chlorosulfonyle

: 109-89-7
diethylamine

: 876403-98-4
N-[(diethylamino)carbonyl]-2,3:4,5-bis-O-(1-methylethylidene)-β-D-fructopyranose sulfamate

Guidance literature:: isocyanate de chlorosulfonyle; diethylamine; In dichloromethane; at -25 - 25 ℃; for 0.5h;

2,3;4,5-di-O-isopropylidene-β-D-fructopyranose; With triethylamine; In dichloromethane; at -25 - 25 ℃; for 3h; Product distribution / selectivity;