2,4-dimethyl-6-[[[2-(dimethylamino)ethyl]amino]methyl]-phenol

Base Information

• Chemical Name: 2,4-dimethyl-6-[[[2-(dimethylamino)ethyl]amino]methyl]-phenol
• CAS No.: 1260396-34-6
• Molecular Formula: C₁₃H₂₂N₂O
• Molecular Weight: 222.33
• Mol file: 1260396-34-6.mol

Synonyms:2,4-dimethyl-6-[[[2-(dimethylamino)ethyl]amino]methyl]-phenol

Chemical Property of 2,4-dimethyl-6-[[[2-(dimethylamino)ethyl]amino]methyl]-phenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2,4-dimethyl-6-[[[2-(dimethylamino)ethyl]amino]methyl]-phenol

There total 2 articles about 2,4-dimethyl-6-[[[2-(dimethylamino)ethyl]amino]methyl]-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3,5-dimethylsalicylaldehyde (24623-61-8) + N,N-dimethylethylenediamine (108-00-9) → 2,4-dimethyl-6-[[[2-(dimethylamino)ethyl]amino]methyl]-phenol (1260396-34-6)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; at 50 ℃; for 24h; under 5250.53 Torr;

DOI:10.1039/c3nj00115f

Reference yield: 40.4%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + N,N-dimethylethylenediamine (108-00-9) + 2,4-Xylenol (105-67-9) → 2,4-dimethyl-6-[[[2-(dimethylamino)ethyl]amino]methyl]-phenol (1260396-34-6)

Guidance literature:

formaldehyd; N,N-dimethylethylenediamine; In methanol; water; for 1h; Reflux;

2,4-Xylenol; In methanol; water; for 72h; Reflux;

DOI:10.1039/c3dt53431f

Reference yield: 17.8%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2,4-di-tert-Butylphenol (96-76-4) + 2,4-dimethyl-6-[[[2-(dimethylamino)ethyl]amino]methyl]-phenol (1260396-34-6) → 2-[[[[3,5-bis(1,1-dimethylethyl)-2-hydroxyphenyl]methyl][2-(dimethylamino)ethyl]amino]methyl]-4,6-dimethylphenol (685859-39-6)

Guidance literature:

In methanol; water; for 96h; Reflux;

DOI:10.1039/c3dt53431f

upstream raw materials:

3,5-dimethylsalicylaldehyde

N,N-dimethylethylenediamine

formaldehyd

2,4-Xylenol

Downstream raw materials:

2-[[[[3,5-bis(1,1-dimethylethyl)-2-hydroxyphenyl]methyl][2-(dimethylamino)ethyl]amino]methyl]-4,6-dimethylphenol