(7-benzyloxy-1-hydroxy-4-methoxy-1,3-dihydro-isobenzofuran-1-yl)-acetic acid tert-butyl ester

Base Information

• Chemical Name: (7-benzyloxy-1-hydroxy-4-methoxy-1,3-dihydro-isobenzofuran-1-yl)-acetic acid tert-butyl ester
• CAS No.: 308277-81-8
• Molecular Formula: C₂₂H₂₆O₆
• Molecular Weight: 386.445

Synonyms:(7-benzyloxy-1-hydroxy-4-methoxy-1,3-dihydro-isobenzofuran-1-yl)-acetic acid tert-butyl ester

Chemical Property of (7-benzyloxy-1-hydroxy-4-methoxy-1,3-dihydro-isobenzofuran-1-yl)-acetic acid tert-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (7-benzyloxy-1-hydroxy-4-methoxy-1,3-dihydro-isobenzofuran-1-yl)-acetic acid tert-butyl ester

There total 1 articles about (7-benzyloxy-1-hydroxy-4-methoxy-1,3-dihydro-isobenzofuran-1-yl)-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

acetic acid tert-butyl ester (540-88-5) + 7-benzyloxy-4-methoxy-3H-isobenzofuran-1-one → (7-benzyloxy-1-hydroxy-4-methoxy-1,3-dihydro-isobenzofuran-1-yl)-acetic acid tert-butyl ester (308277-81-8)

Guidance literature:

acetic acid tert-butyl ester; With lithium diisopropyl amide;

7-benzyloxy-4-methoxy-3H-isobenzofuran-1-one; Further stages.;

DOI:10.1021/ol006531+

Reference yield: 95.0%

(7-benzyloxy-1-hydroxy-4-methoxy-1,3-dihydro-isobenzofuran-1-yl)-acetic acid tert-butyl ester (308277-81-8) → (7-benzyloxy-4-methoxy-1,3-dihydro-isobenzofuran-1-yl)-acetic acid (308277-95-4)

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane;

DOI:10.1021/ol006531+

Reference yield: 88.0%

methanol (67-56-1) + (7-benzyloxy-1-hydroxy-4-methoxy-1,3-dihydro-isobenzofuran-1-yl)-acetic acid tert-butyl ester (308277-81-8) → (7-benzyloxy-1,4-dimethoxy-1,3-dihydro-isobenzofuran-1-yl)-acetic acid tert-butyl ester

Guidance literature:

With Amberlite IR 120(plus); for 0.0833333h;

DOI:10.1021/ol006531+

upstream raw materials:

acetic acid tert-butyl ester

Downstream raw materials:

(7-benzyloxy-4-methoxy-1,3-dihydro-isobenzofuran-1-yl)-acetic acid

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