Cyclohexanecarboxylic acid, 4-amino-, methyl ester (9CI)

Base Information

• Chemical Name: Cyclohexanecarboxylic acid, 4-amino-, methyl ester (9CI)
• CAS No.: 175867-59-1
• Molecular Formula: C8H15 N O2
• Molecular Weight: 157.213
• Hs Code.: 2922499990
• Mol file: 175867-59-1.mol

Synonyms:4-Aminocyclohexanecarboxylicacid methyl ester; Methyl 4-aminocyclohexanecarboxylate

Chemical Property of Cyclohexanecarboxylic acid, 4-amino-, methyl ester (9CI)

Chemical Property:

• PSA: 52.32000
• LogP: 1.37720

Purity/Quality:

97% ^*data from raw suppliers

Methyl 4-aminocyclohexanecarboxylate 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxylic acid, 4-amino-, methyl ester (9CI)

There total 8 articles about Cyclohexanecarboxylic acid, 4-amino-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

methanol (67-56-1) + 4-aminocyclohexanecarboxylic acid (1776-53-0) → methyl 4-aminocyclohexane-1-carboxylate (175867-59-1)

Guidance literature:

4-aminocyclohexanecarboxylic acid; With thionyl chloride; In dichloromethane; at 20 ℃; for 0.666667h;

methanol; for 2.25h; Heating / reflux;

With sodium hydroxide; In water;

Reference yield:

methyl 4-(benzylamino)cyclohexane-1-carboxylate → methyl 4-aminocyclohexane-1-carboxylate (175867-59-1)

Guidance literature:

With 10 wt% Pd(OH)2 on carbon; hydrogen; In methanol; at 20 ℃; for 48h;

Reference yield:

4-aminocyclohexanecarboxylic acid (1776-53-0) → methyl 4-aminocyclohexane-1-carboxylate (175867-59-1)

Guidance literature:

With thionyl chloride; In methanol; Reflux;

upstream raw materials:

methanol

4-aminocyclohexanecarboxylic acid

4-amino-benzoic acid

diazomethyl-trimethyl-silane

Downstream raw materials:

4-dibenzoylaminocyclohexanecarboxylate

methyl (1r,4r)-4-benzamidocyclohexane-1-carboxylate

methyl (1s,4s)-4-benzamidocyclohexane-1-carboxylate

trans methyl 4-(N,N-dibenzylamino)-cyclohexyl-carboxylate

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