(1-hydro-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-ylmethyl)-phosphonic acid monomethyl ester

Base Information

Chemical Name:(1-hydro-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-ylmethyl)-phosphonic acid monomethyl ester
CAS No.:1196474-06-2
Molecular Formula:C₁₅H₁₆BO₆P
Molecular Weight:334.073
Hs Code.:

Synonyms:(1-hydro-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-ylmethyl)-phosphonic acid monomethyl ester

Suppliers and Price of (1-hydro-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-ylmethyl)-phosphonic acid monomethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1-hydro-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-ylmethyl)-phosphonic acid monomethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1-hydro-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-ylmethyl)-phosphonic acid monomethyl ester

There total 5 articles about (1-hydro-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-ylmethyl)-phosphonic acid monomethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 67-56-1
methanol

: 1196474-07-3
(1-hydro-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-ylmethyl)-phosphonic acid dimethyl ester

: 1196474-06-2
(1-hydro-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-ylmethyl)-phosphonic acid monomethyl ester

Guidance literature:: With hydrogenchloride; In water; for 48h; Reflux;

Reference yield:

: 59142-68-6
2-bromo-4-fluorobenzaldehyde

: 1196474-06-2
(1-hydro-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-ylmethyl)-phosphonic acid monomethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 20 - 100 °C

2.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 1.5 h / 80 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C

3.2: -78 - 0 °C

4.1: hydrogenchloride / water / 48 h / Reflux

With hydrogenchloride; n-butyllithium; potassium acetate; potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; hexane; water; N,N-dimethyl-formamide;

Reference yield:

: 1196474-92-6
2-bromo-4-phenoxybenzaldehyde

: 1196474-06-2
(1-hydro-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-ylmethyl)-phosphonic acid monomethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 1.5 h / 80 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C

2.2: -78 - 0 °C

3.1: hydrogenchloride / water / 48 h / Reflux

With hydrogenchloride; n-butyllithium; potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; hexane; water;