2-(4-N-acetylamino-phenacyl)-thio-1,N⁶-etheno-2'-deoxyadenosine 5'-monophosphate

Base Information

• Chemical Name: 2-(4-N-acetylamino-phenacyl)-thio-1,N⁶-etheno-2'-deoxyadenosine 5'-monophosphate
• CAS No.: 419549-36-3
• Molecular Formula: C₂₂H₂₃N₆O₈PS
• Molecular Weight: 562.5

Synonyms:2-(4-N-acetylamino-phenacyl)-thio-1,N⁶-etheno-2'-deoxyadenosine 5'-monophosphate

Chemical Property of 2-(4-N-acetylamino-phenacyl)-thio-1,N⁶-etheno-2'-deoxyadenosine 5'-monophosphate

Chemical Property:

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Technology Process of 2-(4-N-acetylamino-phenacyl)-thio-1,N⁶-etheno-2'-deoxyadenosine 5'-monophosphate

There total 2 articles about 2-(4-N-acetylamino-phenacyl)-thio-1,N⁶-etheno-2'-deoxyadenosine 5'-monophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

4-acetylaminophenacyl bromide (21675-02-5) + triethylammonium 2-thio-1,N6-etheno-2'-deoxyadenosine 5'-monophosphate → 2-(4-N-acetylamino-phenacyl)-thio-1,N6-etheno-2'-deoxyadenosine 5'-monophosphate (419549-36-3)

Guidance literature:

In water; acetonitrile; at 20 ℃; pH=7.0;

DOI:10.1016/S0968-0896(01)00297-8

Reference yield:

4-(N-acetylamino)acetophenone (2719-21-3,150667-24-6) → 2-(4-N-acetylamino-phenacyl)-thio-1,N6-etheno-2'-deoxyadenosine 5'-monophosphate (419549-36-3)

Guidance literature:

Multi-step reaction with 2 steps

1: bromine; toluenesulfonic acid

2: 66 percent / H₂O; acetonitrile / 20 °C / pH 7.0

With o-toluenesulfonic acid; bromine; In water; acetonitrile;

DOI:10.1016/S0968-0896(01)00297-8

Reference yield: 31.0%

2-(4-N-acetylamino-phenacyl)-thio-1,N6-etheno-2'-deoxyadenosine 5'-monophosphate (419549-36-3) → 2-(4-N-acetylamino-phenylacyl)thio-1,N6-etheno-2'-deoxyadenosine 5'-triphosphate

Guidance literature:

2-(4-N-acetylamino-phenacyl)-thio-1,N⁶-etheno-2'-deoxyadenosine 5'-monophosphate; With tributyl-amine; chlorophosphoric acid diphenyl ester; In 1,4-dioxane;

With pyridine; tri(n-butyl)ammonium pyrophosphate;

DOI:10.1016/S0968-0896(01)00297-8

upstream raw materials:

4-acetylaminophenacyl bromide

4-(N-acetylamino)acetophenone

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