N'-(4-iodophenyl)-N-[4-(trifluoromethyl)phenyl]-4-benzyloxybenzenecarbohydrazonamide

Base Information

Chemical Name:N'-(4-iodophenyl)-N-[4-(trifluoromethyl)phenyl]-4-benzyloxybenzenecarbohydrazonamide
CAS No.:1621377-85-2
Molecular Formula:C₂₇H₂₁F₃IN₃O
Molecular Weight:587.383
Hs Code.:

Synonyms:N'-(4-iodophenyl)-N-[4-(trifluoromethyl)phenyl]-4-benzyloxybenzenecarbohydrazonamide

Suppliers and Price of N'-(4-iodophenyl)-N-[4-(trifluoromethyl)phenyl]-4-benzyloxybenzenecarbohydrazonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(4-iodophenyl)-N-[4-(trifluoromethyl)phenyl]-4-benzyloxybenzenecarbohydrazonamide

Chemical Property:

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Technology Process of N'-(4-iodophenyl)-N-[4-(trifluoromethyl)phenyl]-4-benzyloxybenzenecarbohydrazonamide

There total 4 articles about N'-(4-iodophenyl)-N-[4-(trifluoromethyl)phenyl]-4-benzyloxybenzenecarbohydrazonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1621377-97-6
C₂₁H₁₅ClF₃NO

: 13116-27-3
4-iodophenylhydrazine

: 1621377-85-2
N'-(4-iodophenyl)-N-[4-(trifluoromethyl)phenyl]-4-benzyloxybenzenecarbohydrazonamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo500898e

Reference yield:

: 1486-50-6
4-(benzyloxy)benzoic acid chloride

: 1621377-85-2
N'-(4-iodophenyl)-N-[4-(trifluoromethyl)phenyl]-4-benzyloxybenzenecarbohydrazonamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: thionyl chloride / Inert atmosphere; Reflux

3: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jo500898e

Reference yield:

: 1621377-94-3
4-benzyloxy-N-(4-(trifluoromethyl)phenyl)benzamide

: 1621377-85-2
N'-(4-iodophenyl)-N-[4-(trifluoromethyl)phenyl]-4-benzyloxybenzenecarbohydrazonamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / Inert atmosphere; Reflux

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jo500898e