[(S)-2-(1-Methoxy-1-methyl-ethyl)-pyrrolidin-1-yl]-phosphonic acid butyl ester 2,4-dichloro-phenyl ester

Base Information

• Chemical Name: [(S)-2-(1-Methoxy-1-methyl-ethyl)-pyrrolidin-1-yl]-phosphonic acid butyl ester 2,4-dichloro-phenyl ester
• CAS No.: 129149-63-9
• Molecular Formula: C₁₈H₂₈Cl₂NO₄P
• Molecular Weight: 424.304

Synonyms:[(S)-2-(1-Methoxy-1-methyl-ethyl)-pyrrolidin-1-yl]-phosphonic acid butyl ester 2,4-dichloro-phenyl ester

Chemical Property of [(S)-2-(1-Methoxy-1-methyl-ethyl)-pyrrolidin-1-yl]-phosphonic acid butyl ester 2,4-dichloro-phenyl ester

Chemical Property:

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Technology Process of [(S)-2-(1-Methoxy-1-methyl-ethyl)-pyrrolidin-1-yl]-phosphonic acid butyl ester 2,4-dichloro-phenyl ester

There total 1 articles about [(S)-2-(1-Methoxy-1-methyl-ethyl)-pyrrolidin-1-yl]-phosphonic acid butyl ester 2,4-dichloro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[(S)-2-(1-Methoxy-1-methyl-ethyl)-pyrrolidin-1-yl]-phosphonic acid bis-(2,4-dichloro-phenyl) ester (129149-60-6) + butan-1-ol (71-36-3) → [(S)-2-(1-Methoxy-1-methyl-ethyl)-pyrrolidin-1-yl]-phosphonic acid butyl ester 2,4-dichloro-phenyl ester (129149-63-9)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) THF, hexane, 0 deg C, 2.) 0 deg C, 1 h;

DOI:10.1021/ja00175a030

Reference yield: 74.0%

methanol (67-56-1) + [(S)-2-(1-Methoxy-1-methyl-ethyl)-pyrrolidin-1-yl]-phosphonic acid butyl ester 2,4-dichloro-phenyl ester (129149-63-9) → (S)-butyl 2,4-dichlorophenyl methyl phosphate (129149-64-0)

Guidance literature:

With hydrogenchloride; Ambient temperature;

DOI:10.1021/ja00175a030

upstream raw materials:

[(S)-2-(1-Methoxy-1-methyl-ethyl)-pyrrolidin-1-yl]-phosphonic acid bis-(2,4-dichloro-phenyl) ester

butan-1-ol

Downstream raw materials:

(S)-butyl 2,4-dichlorophenyl methyl phosphate

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