C₂₂H₃₉N₃O₁₂S₂*C₇H₈O₃S

Base Information

• Chemical Name: C₂₂H₃₉N₃O₁₂S₂*C₇H₈O₃S
• CAS No.: 1415712-84-3
• Molecular Formula: C₇H₈O₃S*C₂₂H₃₉N₃O₁₂S₂
• Molecular Weight: 773.901
• Mol file: 1415712-84-3.mol

Synonyms:C₂₂H₃₉N₃O₁₂S₂*C₇H₈O₃S

Chemical Property of C₂₂H₃₉N₃O₁₂S₂*C₇H₈O₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₃₉N₃O₁₂S₂*C₇H₈O₃S

There total 7 articles about C₂₂H₃₉N₃O₁₂S₂*C₇H₈O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-(2-aminoethoxy)ethoxy)ethan-1-ol (6338-55-2) → C22H39N3O12S2*C7H8O3S (1415712-84-3)

Guidance literature:

Multi-step reaction with 6 steps

1.1: sodium hydrogencarbonate / water; acetonitrile / 2 h / 0 - 20 °C / Inert atmosphere

2.1: potassium hydrogencarbonate / acetonitrile / 72 h / 80 °C / Inert atmosphere

3.1: sodium iodide / acetone / 20 h / 20 °C / Inert atmosphere

3.2: polymer-supported triphenylphosphine / 1.67 h / 0 - 20 °C / Inert atmosphere

3.3: 4.17 h / 0 - 20 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

4.2: 0.83 h / 0 - 20 °C / Inert atmosphere

5.1: potassium permanganate / water; acetic acid / 1 h / -15 - -10 °C / Inert atmosphere

6.1: palladium on activated charcoal; hydrogen / ethanol; ethyl acetate / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

With potassium permanganate; palladium on activated charcoal; hydrogen; sodium hydrogencarbonate; potassium hydrogencarbonate; triethylamine; sodium iodide; In ethanol; dichloromethane; water; acetic acid; ethyl acetate; acetone; acetonitrile; 2.1: |Michael Addition;

DOI:10.1016/j.tet.2011.10.100

Reference yield:

(2S,5R,6R)-2-[(2,2-dimethylpropanoyl)oxy]-methylpenicillanat-6-aminium 4-methylbenzenesulfonate (25031-03-2) → C22H39N3O12S2*C7H8O3S (1415712-84-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 0.83 h / 0 - 20 °C / Inert atmosphere

2.1: potassium permanganate / water; acetic acid / 1 h / -15 - -10 °C / Inert atmosphere

3.1: palladium on activated charcoal; hydrogen / ethanol; ethyl acetate / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

With potassium permanganate; palladium on activated charcoal; hydrogen; triethylamine; In ethanol; dichloromethane; water; acetic acid; ethyl acetate;

DOI:10.1016/j.tet.2011.10.100

Reference yield:

C16H24ClNO7S (1415712-78-5) → C22H39N3O12S2*C7H8O3S (1415712-84-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 0.83 h / 0 - 20 °C / Inert atmosphere

2.1: potassium permanganate / water; acetic acid / 1 h / -15 - -10 °C / Inert atmosphere

3.1: palladium on activated charcoal; hydrogen / ethanol; ethyl acetate / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

With potassium permanganate; palladium on activated charcoal; hydrogen; triethylamine; In ethanol; dichloromethane; water; acetic acid; ethyl acetate;

DOI:10.1016/j.tet.2011.10.100

upstream raw materials:

(2S,5R,6R)-2-[(2,2-dimethylpropanoyl)oxy]-methylpenicillanat-6-aminium 4-methylbenzenesulfonate

C₃₀H₄₅N₃O₁₂S₂

2-[2-{2-(N-benzyloxycarbonyl)aminoethoxy}ethoxy]ethanol

C₁₈H₂₉NO₈S