tert-butyl-(6-[1,3]dithian-2-yl-4-methyl-hex-3-enyloxy)-diphenyl-silane

Base Information

Chemical Name:tert-butyl-(6-[1,3]dithian-2-yl-4-methyl-hex-3-enyloxy)-diphenyl-silane
CAS No.:226879-33-0
Molecular Formula:C₂₇H₃₈OS₂Si
Molecular Weight:470.816
Hs Code.:

<i>tert</i>-butyl-(6-[1,3]dithian-2-yl-4-methyl-hex-3-enyloxy)-diphenyl-silane

Synonyms:tert-butyl-(6-[1,3]dithian-2-yl-4-methyl-hex-3-enyloxy)-diphenyl-silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl-(6-[1,3]dithian-2-yl-4-methyl-hex-3-enyloxy)-diphenyl-silane

Chemical Property:

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Technology Process of tert-butyl-(6-[1,3]dithian-2-yl-4-methyl-hex-3-enyloxy)-diphenyl-silane

There total 5 articles about tert-butyl-(6-[1,3]dithian-2-yl-4-methyl-hex-3-enyloxy)-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 109-80-8
1.3-propanedithiol

: 226879-32-9
(E)-4-methyl-7-(tert-butyldiphenylsilyl)oxyhept-3-en-1-al

: 226879-33-0
tert-butyl-(6-[1,3]dithian-2-yl-4-methyl-hex-3-enyloxy)-diphenyl-silane

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/S0040-4039(99)00323-8

Reference yield:

: 112897-03-7
3-(tert-butyldiphenylsilyloxy)-1-propanal

: 226879-33-0
tert-butyl-(6-[1,3]dithian-2-yl-4-methyl-hex-3-enyloxy)-diphenyl-silane

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / diethyl ether

2: 80 percent / PrCOOH / 140 °C

3: 95 percent / DIBALH / CH₂Cl₂

4: 80 percent / BF₃*Et₂O / CH₂Cl₂

With boron trifluoride diethyl etherate; diisobutylaluminium hydride; butyric acid; In diethyl ether; dichloromethane; 1: Grignard reaction / 2: Condensation / 3: Reduction / 4: Condensation;
DOI:10.1016/S0040-4039(99)00323-8

Reference yield:

: 127047-71-6
3-(tert-butyldiphenylsilyloxy)propan-1-ol

: 226879-33-0
tert-butyl-(6-[1,3]dithian-2-yl-4-methyl-hex-3-enyloxy)-diphenyl-silane

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / (COCl)2; Et₃N; DMSO / CH₂Cl₂ / -78 °C

2: 80 percent / diethyl ether

3: 80 percent / PrCOOH / 140 °C

4: 95 percent / DIBALH / CH₂Cl₂

5: 80 percent / BF₃*Et₂O / CH₂Cl₂

With oxalyl dichloride; boron trifluoride diethyl etherate; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; butyric acid; In diethyl ether; dichloromethane; 1: Oxidation / 2: Grignard reaction / 3: Condensation / 4: Reduction / 5: Condensation;
DOI:10.1016/S0040-4039(99)00323-8