1-cyclohexyl-2-propynyl pentafluorobenzoate

Base Information

• Chemical Name: 1-cyclohexyl-2-propynyl pentafluorobenzoate
• CAS No.: 1291103-55-3
• Molecular Formula: C₁₆H₁₃F₅O₂
• Molecular Weight: 332.27
• Mol file: 1291103-55-3.mol

Synonyms:1-cyclohexyl-2-propynyl pentafluorobenzoate

Chemical Property of 1-cyclohexyl-2-propynyl pentafluorobenzoate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1-cyclohexyl-2-propynyl pentafluorobenzoate

There total 1 articles about 1-cyclohexyl-2-propynyl pentafluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pentafluorobenzoylchloride (2251-50-5) + cyclohexanecarbaldehyde (2043-61-0) → 1-cyclohexyl-2-propynyl pentafluorobenzoate (1291103-55-3)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol200703g

Reference yield: 76.0%

Allylbenzylamine (4383-22-6) + 1-cyclohexyl-2-propynyl pentafluorobenzoate (1291103-55-3) → C19H25N

Guidance literature:

With C₃₁H₂₆N₃P; copper(II) acetate monohydrate; N-ethyl-N,N-diisopropylamine; In methanol; at -20 ℃; enantioselective reaction;

DOI:10.1039/d0ra07698h

Reference yield: 65.0%

1-cyclohexyl-2-propynyl pentafluorobenzoate (1291103-55-3) + methyl 3-oxo-3-phenylpropionate (614-27-7) → (R)-methyl 4-cyclohexyl-5-methylene-2-phenyl-4,5-dihydrofuran-3-carboxylate

Guidance literature:

With C₃₂H₂₇N₂P; copper(II) bis(trifluoromethanesulfonate); triethylamine; In methanol; at 20 ℃; for 24h; enantioselective reaction; Schlenk technique; Inert atmosphere;

DOI:10.1002/anie.201405857

upstream raw materials:

pentafluorobenzoylchloride

cyclohexanecarbaldehyde

Downstream raw materials:

1-(1-cyclohexyl-2-propyn-1-yl)indoline

4-methyl-N-(1-cyclohexyl-2-propynyl)-N-methylaniline

4-chloro-N-(1-cyclohexyl-2-propynyl)-N-methylaniline

N-(1-cyclohexyl-2-propynyl)aniline