allyl 4-acetoxy-4-benzyl-3-[2-(2-bromophenyl)ethylsulfanyl]-5-phenylpentanoate

Base Information

Chemical Name:allyl 4-acetoxy-4-benzyl-3-[2-(2-bromophenyl)ethylsulfanyl]-5-phenylpentanoate
CAS No.:697745-48-5
Molecular Formula:C₃₁H₃₃BrO₄S
Molecular Weight:581.571
Hs Code.:

Synonyms:allyl 4-acetoxy-4-benzyl-3-[2-(2-bromophenyl)ethylsulfanyl]-5-phenylpentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 4-acetoxy-4-benzyl-3-[2-(2-bromophenyl)ethylsulfanyl]-5-phenylpentanoate

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Technology Process of allyl 4-acetoxy-4-benzyl-3-[2-(2-bromophenyl)ethylsulfanyl]-5-phenylpentanoate

There total 4 articles about allyl 4-acetoxy-4-benzyl-3-[2-(2-bromophenyl)ethylsulfanyl]-5-phenylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 697745-47-4
allyl 4-acetoxy-4-benzyl-5-phenyl-2E-pentenoate

: 24084-15-9
2-(2'-bromophenyl)ethanethiol

: 697745-48-5
allyl 4-acetoxy-4-benzyl-3-[2-(2-bromophenyl)ethylsulfanyl]-5-phenylpentanoate

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 20 ℃;
DOI:10.1139/v03-148

Reference yield:

: 697745-46-3
2-acetoxy-2-benzyldihydrocinnamaldehyde

: 697745-48-5
allyl 4-acetoxy-4-benzyl-3-[2-(2-bromophenyl)ethylsulfanyl]-5-phenylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / benzene / Heating

2: 24 percent / NaH / dimethylsulfoxide / 20 °C

With sodium hydride; In dimethyl sulfoxide; benzene; 1: Wittig olefination;
DOI:10.1139/v03-148

Reference yield:

: 22859-80-9
2-benzyl-3-phenylpropionaldehyde

: 697745-48-5
allyl 4-acetoxy-4-benzyl-3-[2-(2-bromophenyl)ethylsulfanyl]-5-phenylpentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent / BF₃*OEt₂ / benzene / 20 °C

2: 54 percent / benzene / Heating

3: 24 percent / NaH / dimethylsulfoxide / 20 °C

With boron trifluoride diethyl etherate; sodium hydride; In dimethyl sulfoxide; benzene; 2: Wittig olefination;
DOI:10.1139/v03-148