(1R,3S,5S,6R,8S)-3,8-dimethyl-2,4,7,9-tetraoxabicyclo<4.4.2>dec-5-ylmethanol

Base Information

Chemical Name:(1R,3S,5S,6R,8S)-3,8-dimethyl-2,4,7,9-tetraoxabicyclo<4.4.2>dec-5-ylmethanol
CAS No.:212121-56-7
Molecular Formula:C₉H₁₆O₅
Molecular Weight:204.223
Hs Code.:

Synonyms:(1R,3S,5S,6R,8S)-3,8-dimethyl-2,4,7,9-tetraoxabicyclo<4.4.2>dec-5-ylmethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,3S,5S,6R,8S)-3,8-dimethyl-2,4,7,9-tetraoxabicyclo<4.4.2>dec-5-ylmethanol

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Technology Process of (1R,3S,5S,6R,8S)-3,8-dimethyl-2,4,7,9-tetraoxabicyclo<4.4.2>dec-5-ylmethanol

There total 3 articles about (1R,3S,5S,6R,8S)-3,8-dimethyl-2,4,7,9-tetraoxabicyclo<4.4.2>dec-5-ylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1-O-acetyl-2,4:3,5-di-O-ethylidene-DL-xylitol

: 212121-56-7,7473-46-3
(1R,3S,5S,6R,8S)-3,8-dimethyl-2,4,7,9-tetraoxabicyclo<4.4.2>dec-5-ylmethanol

Guidance literature:: With phosphate buffer; In water; at 20 ℃; for 19h;
DOI:10.1016/S0040-4020(98)01174-0

Reference yield:

: 87-99-0
XYLITOL

: 212121-56-7,7473-46-3
(1R,3S,5S,6R,8S)-3,8-dimethyl-2,4,7,9-tetraoxabicyclo<4.4.2>dec-5-ylmethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / HCl / H₂O / 3 h / 50 °C

2: 96 percent / DMAP / pyridine / 16 h / 20 °C

3: 86 percent / PPL, phosphate buffer / H₂O / 19 h / 20 °C

With hydrogenchloride; dmap; phosphate buffer; In pyridine; water;
DOI:10.1016/S0040-4020(98)01174-0

Reference yield:

: 7473-46-3
2,4:3,5-di-O-ethylidene-DL-xylitol

: 212121-56-7,7473-46-3
(1R,3S,5S,6R,8S)-3,8-dimethyl-2,4,7,9-tetraoxabicyclo<4.4.2>dec-5-ylmethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / DMAP / pyridine / 16 h / 20 °C

2: 86 percent / PPL, phosphate buffer / H₂O / 19 h / 20 °C

With dmap; phosphate buffer; In pyridine; water;
DOI:10.1016/S0040-4020(98)01174-0