(E)-2-(Cyclohexanecarboximidoyl-aminooxy)-but-2-enedioic acid dimethyl ester

Base Information

Chemical Name:(E)-2-(Cyclohexanecarboximidoyl-aminooxy)-but-2-enedioic acid dimethyl ester
CAS No.:878650-01-2
Molecular Formula:C₁₃H₂₀N₂O₅
Molecular Weight:284.312
Hs Code.:

Synonyms:(E)-2-(Cyclohexanecarboximidoyl-aminooxy)-but-2-enedioic acid dimethyl ester

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Chemical Property of (E)-2-(Cyclohexanecarboximidoyl-aminooxy)-but-2-enedioic acid dimethyl ester

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Technology Process of (E)-2-(Cyclohexanecarboximidoyl-aminooxy)-but-2-enedioic acid dimethyl ester

There total 2 articles about (E)-2-(Cyclohexanecarboximidoyl-aminooxy)-but-2-enedioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 762-42-5
dimethyl acetylenedicarboxylate

: 633313-98-1
N'-hydroxycyclohexanecarboximidamide

: 878650-01-2
(E)-2-(Cyclohexanecarboximidoyl-aminooxy)-but-2-enedioic acid dimethyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 3h; Heating;
DOI:10.1021/jm051064t

Reference yield:

: 766-05-2
cyclohexane carbonitrile

: 878650-01-2
(E)-2-(Cyclohexanecarboximidoyl-aminooxy)-but-2-enedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NH₂OH*HCl; Na₂CO₃ / ethanol; H₂O / 24 h / 20 °C

2: 91 percent / Et₃N / CH₂Cl₂ / 3 h / Heating

With hydroxylamine hydrochloride; sodium carbonate; triethylamine; In ethanol; dichloromethane; water;
DOI:10.1021/jm051064t