Technology Process of C15H20O5
There total 6 articles about C15H20O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C12H14O3;
With
methanesulfonamide; AD-mix β;
In
water; tert-butyl alcohol;
at 0 ℃;
Inert atmosphere;
2,2-dimethoxy-propane;
With
toluene-4-sulfonic acid;
In
acetone;
at 20 ℃;
for 1h;
optical yield given as %ee;
chemoselective reaction;
Inert atmosphere;
DOI:10.1021/ja107190w
- Guidance literature:
-
With
pyridinium p-toluenesulfonate;
In
acetone;
at 20 ℃;
for 1h;
chemoselective reaction;
Inert atmosphere;
DOI:10.1021/ja2041964
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium dihydrogenphosphate; disodium hydrogenphosphate / water / 8 h / 100 °C / Inert atmosphere
2.1: potassium hexacyanoferrate (III); (DHQD)2PHAL; potassium osmate; methanesulfonamide; potassium carbonate / water; tert-butyl alcohol / 0 °C / Inert atmosphere
2.2: 0.67 h / 20 °C / Inert atmosphere
3.1: pyridinium p-toluenesulfonate / acetone / 1 h / 20 °C / Inert atmosphere
With
1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; potassium hexacyanoferrate (III); disodium hydrogenphosphate; sodium dihydrogenphosphate; (DHQD)2PHAL; potassium osmate; methanesulfonamide; pyridinium p-toluenesulfonate; potassium carbonate;
In
water; acetone; tert-butyl alcohol;
2.1: Sharpless dihydroxylation;
DOI:10.1021/ja2041964
