6-(2-hydroxyethyl)hept-6-en-4-ynoic acid (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl ester

Base Information

Chemical Name:6-(2-hydroxyethyl)hept-6-en-4-ynoic acid (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl ester
CAS No.:732284-15-0
Molecular Formula:C₁₉H₃₀O₃
Molecular Weight:306.445
Hs Code.:

Synonyms:6-(2-hydroxyethyl)hept-6-en-4-ynoic acid (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl ester

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Chemical Property of 6-(2-hydroxyethyl)hept-6-en-4-ynoic acid (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl ester

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Technology Process of 6-(2-hydroxyethyl)hept-6-en-4-ynoic acid (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl ester

There total 3 articles about 6-(2-hydroxyethyl)hept-6-en-4-ynoic acid (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 76334-36-6
3-bromobut-3-en-1-ol

: 732284-14-9
pent-4-ynoic acid (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl ester

: 732284-15-0
6-(2-hydroxyethyl)hept-6-en-4-ynoic acid (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl ester

Guidance literature:: With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 20 ℃; for 17h;
DOI:10.1002/adsc.200303201

Reference yield:

: 2216-51-5
(-)-menthol

: 732284-15-0
6-(2-hydroxyethyl)hept-6-en-4-ynoic acid (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 4-toluenesulfonic acid monohydrate / CCl₄ / 20 h / Heating

2: 86 percent / Et₃N; CuI / (PPh₃)2PdCl₂ / tetrahydrofuran / 17 h / 20 °C

With copper(l) iodide; p-toluenesulfonic acid monohydrate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; tetrachloromethane; 2: Sonogashira coupling;
DOI:10.1002/adsc.200303201

Reference yield:

: 6089-09-4
4-pentynoic acid

: 732284-15-0
6-(2-hydroxyethyl)hept-6-en-4-ynoic acid (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 4-toluenesulfonic acid monohydrate / CCl₄ / 20 h / Heating

2: 86 percent / Et₃N; CuI / (PPh₃)2PdCl₂ / tetrahydrofuran / 17 h / 20 °C

With copper(l) iodide; p-toluenesulfonic acid monohydrate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; tetrachloromethane; 2: Sonogashira coupling;
DOI:10.1002/adsc.200303201